Synthesis, biocompatible, and self-assembly properties of poly (ethylene glycol)/lactobionic acid-grafted chitosan

J Biomater Sci Polym Ed. 2014 Jul;25(10):1062-75. doi: 10.1080/09205063.2014.918465. Epub 2014 May 21.

Abstract

Polymers with targeted ligands are widely used as the anti-cancer drug delivery materials. For applications of chitosan as an anti-liver cancer drug delivery, poly (ethylene glycol)/lactobionic acid-grafted chitosan (PEG/LA-CS) was prepared and investigated since lactobionic acid can be specifically recognized by the hepatocytes. The structure of the PEG/LA-CS was characterized by Fourier transform infrared spectrometry and elemental analysis. The self-assembly behaviors of the PEG/LA-CS were monitored by steady-state fluorescence spectroscopy and electronic transmission microscope. The protein adsorption of the PEG/LA-CS was detected with bovine serum albumin (BSA) by electrochemical impedance spectroscopy. The results showed that the PEG/LA-CS almost did not adsorb protein. To study the effects of PEG/LA-CS on the structure of BSA, the interactions between the PEG/LA-CS and BSA were detected by ultraviolet spectrum, fluorescence spectrum, and circular dichroism. All the data gave one result that BSA maintained its original folded confirmation in PEG/LA-CS solution. The hemocompatibility of PEG/LA-CS was investigated by observing the effects of PEG/LA-CS on the hemolysis rate and the plasma recalcification time (PRT). The results showed that the PRT was prolonged greatly and the hemolysis rate was less than 5%. Furthermore, PEG/LA-CS also showed good cytocompatibility with K562, Hep G2, and LO2 cells. Therefore, the PEG/LA-CS is believed to have great potential for producing injectable anti-liver cancer drug delivery.

Keywords: PEG/LA-CS; cytocompatibility; electrochemical impedance spectroscopy; hemocompatibility; self-assembly.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adsorption
  • Animals
  • Biocompatible Materials / chemical synthesis*
  • Biocompatible Materials / chemistry
  • Biocompatible Materials / toxicity*
  • Blood Coagulation / drug effects
  • Cattle
  • Cell Line
  • Cell Survival / drug effects
  • Chemistry Techniques, Synthetic
  • Chitosan / chemistry*
  • Disaccharides / chemistry*
  • Hemolysis / drug effects
  • Humans
  • Materials Testing*
  • Polyethylene Glycols / chemistry*
  • Serum Albumin, Bovine / chemistry
  • Solubility

Substances

  • Biocompatible Materials
  • Disaccharides
  • Serum Albumin, Bovine
  • Polyethylene Glycols
  • lactobionic acid
  • Chitosan