Effect of light curing protocol on degree of conversion of composites

Acta Odontol Scand. 2014 Nov;72(8):898-902. doi: 10.3109/00016357.2014.920108. Epub 2014 May 26.

Abstract

Objective: To evaluate the degree of conversion (DC) of two light-cured composites with different protocols of light curing.

Materials and methods: One hundred and ninety two specimens (n = 8) were prepared (5 mm × 2 mm) according to experimental groups: two composite resins (Filtek Supreme and four seasons); three light curing protocols [20 s with the tip of the light curing unit (LCU) device touching composite surface (C); 20 s with the tip of the LCU at 8 mm distant from composite surface (D); and tip of the LCU at 8 mm distant from composite surface and polymerization time required to obtain a radiant exposure of 16 J/cm(2) (DS)]. Four LCUs (Bluephase 16i, Ultralume LED 5, XL 3000 and Optilux 501C) were used. DC of the bottom and top surface of specimens were measured using a FTIR spectrometer. Data were statistically analyzed by 3-way split splot ANOVA and Tukey's test (alpha = 0.05).

Results: The results showed that DC of the top surface was higher than the bottom at all experimental conditions (p < 0.0001). Overall, the curing at 8 mm of distance did not affect conversion rate on the top surface (p > 0.05), but bottom surfaces showed DC reduction (p < 0.05). The highest monomer conversion values were observed for C and DS situations.

Conclusion: The distance between the LCU and material surface and radiant exposure can affect the DC. Polymerization at distance should be performed with curing units with higher light power and/or extended exposure time.

Keywords: composite resin; degree of conversion; polymerization.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Composite Resins / chemistry
  • Composite Resins / radiation effects*
  • Curing Lights, Dental / classification
  • Dental Materials / chemistry
  • Dental Materials / radiation effects*
  • Humans
  • Light-Curing of Dental Adhesives / instrumentation
  • Light-Curing of Dental Adhesives / methods*
  • Materials Testing
  • Polymerization
  • Random Allocation
  • Spectroscopy, Fourier Transform Infrared
  • Surface Properties
  • Temperature
  • Time Factors

Substances

  • Composite Resins
  • Dental Materials
  • Filtek Supreme
  • flowable hybrid composite