Enhanced dual contrast agent, Co(2+)-doped NaYF4:Yb(3+),Tm(3+) nanorods, for near infrared-to-near infrared upconversion luminescence and magnetic resonance imaging

Biomaterials. 2014 Nov;35(33):9167-76. doi: 10.1016/j.biomaterials.2014.07.031. Epub 2014 Aug 6.

Abstract

Dual-modality imaging with magnetic resonance (MR) and upconversion luminescence (UCL) is a promising technique for molecular imaging in biomedical research. Multifunctional lanthanide-based nanoparticles have been widely investigated as agents for contrast enhanced MR and fluorescence imaging. However, the use of rare earth fluoride nanoparticles for dual-modality imaging of T2-weighted MR and UCL is rarely reported. We find that NaYF4:Yb(3+),Tm(3+),Co(2+) (MUC) nanorods can be applied as a high-performance dual contrast agent for both T2-weighted MR and UCL dual-modality imaging. After modification with 6-O-carboxymethyl chitosan (OCC), MUC nanorods can be endocytosed by cells without showing signs of cytotoxicity. High-quality UCL images of living cells incubated with MUC-OCC nanorods were acquired on a near-infrared (NIR) confocal microscopy under the excitation at 980 nm. Moreover, MUC-OCC nanorods display high transverse (r2) relaxivities in vitro. The application of low-dose MUC-OCC nanorods for NIR-to-NIR UCL and MR dual-modality in vivo imaging was also carried out successfully. In addition, the toxicity of MUC-OCC nanorods was evaluated by MTT assay, serological tests and histological analysis of visceral organs.

Keywords: Lanthanide nanoparticle; Magnetic resonance imaging; Multi-modality imaging; Nanorod; Rare earth nanomaterials; Upconversion luminescence.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Cell Line, Tumor
  • Cell Survival
  • Chitosan / analogs & derivatives
  • Chitosan / chemistry
  • Contrast Media / chemistry*
  • Female
  • Hep G2 Cells
  • Humans
  • Lanthanoid Series Elements / chemistry
  • Luminescence*
  • Magnetic Resonance Imaging / methods*
  • Mice
  • Mice, Nude
  • Microscopy, Confocal / methods
  • Nanoparticles / chemistry
  • Nanotubes / chemistry*
  • Spectroscopy, Near-Infrared / methods*
  • Toxicity Tests

Substances

  • Contrast Media
  • Lanthanoid Series Elements
  • O-carboxymethylchitosan
  • Chitosan