Preparation and characterization of antiadhesion barrier film from hyaluronic acid-grafted electrospun poly(caprolactone) nanofibrous membranes for prevention of flexor tendon postoperative peritendinous adhesion

Int J Nanomedicine. 2014 Aug 22:9:4079-92. doi: 10.2147/IJN.S67931. eCollection 2014.

Abstract

Peritendinous adhesion is one of the common complications encountered after tendon injury and subsequent surgery, and it can be minimized by introducing a physical barrier between the injured site and the surrounding tissue. An electrospun hyaluronic acid-grafted poly(caprolactone) (PCL-g-HA) nanofibrous membrane (NFM) is proposed as an alternative to current antiadhesion barrier films. HA is covalently grafted to surface-aminolyzed PCL nanofibers, using carbodiimide as the coupling agent. Pristine PCL and PCL-g-HA NFMs were characterized by scanning electron microscopy, thermogravimetric analysis, X-ray photoelectron spectroscopy, Fourier-transform infrared spectroscopy, and mechanical testing. In vitro cell culture with fibroblasts showed that PCL-g-HA NFMs reduced cellular adhesion on the membrane surface while maintaining cell proliferation. Animal experiments using a rabbit flexor digitorum profundus tendon model confirmed the efficacy of PCL-g-HA in reducing peritendinous adhesion, based on gross observation, histology, joint flexion-angle measurements, gliding tests, and biomechanical evaluation.

Keywords: antiadhesion; barrier film; hyaluronic acid; nanofibrous membranes; peritendinous adhesion; polycaprolactone; surface grafting.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Cell Adhesion / drug effects
  • Cell Line
  • Cell Survival / drug effects
  • Humans
  • Hyaluronic Acid / chemistry
  • Hyaluronic Acid / pharmacology*
  • Hyaluronic Acid / therapeutic use
  • Male
  • Membranes, Artificial*
  • Nanofibers / chemistry*
  • Nanofibers / therapeutic use
  • Particle Size
  • Polyesters / chemistry
  • Polyesters / pharmacology*
  • Polyesters / therapeutic use
  • Rabbits
  • Tendons / drug effects
  • Tendons / surgery
  • Tissue Adhesions / drug therapy
  • Tissue Adhesions / prevention & control*

Substances

  • Membranes, Artificial
  • Polyesters
  • Seprafilm
  • polycaprolactone
  • Hyaluronic Acid