Development of lipid nanoparticle formulations of siRNA for hepatocyte gene silencing following subcutaneous administration

J Control Release. 2014 Dec 28:196:106-12. doi: 10.1016/j.jconrel.2014.09.025. Epub 2014 Oct 5.

Abstract

Recently developed lipid nanoparticle (LNP) formulations of siRNA have proven to be effective agents for hepatocyte gene silencing following intravenous administration with at least three LNP-siRNA formulations in clinical trials. The aim of this work was to develop LNP-siRNA systems for hepatocyte gene silencing that can be administered subcutaneously (s.c.). Three parameters were investigated, namely LNP size, residence time of the polyethylene glycol (PEG)-lipid coating and the influence of hepatocyte-specific targeting ligands. LNP sizes were varied over the range of 30 to 115 nm in diameter and PEG-lipid that dissociates rapidly (PEG-DMG) and slowly (PEG-DSG) were employed. In mice, results show that large (~80 nm) LNP exhibited limited accumulation in the liver and poor Factor VII (FVII) gene silencing at 1mg siRNA/kg body weight. Conversely, small (~30 nm) LNP systems showed maximal liver accumulation yet still had minimal activity. Interestingly, intermediate size (~45 nm) LNP containing PEG-DSG exhibited nearly equivalent liver accumulation as the smaller systems following s.c. administration but reduced FVII levels by 80% at 1mg siRNA/kg body weight. Smaller systems (~35 nm diameter) containing either PEG-DMG or PEG-DSG were less active; however addition of 0.5 mol.% of a GalNAc-PEG lipid to these smaller systems improved activity to levels similar to that observed for the ~45 nm diameter systems. In summary, this work shows that appropriately designed LNP-siRNA systems can result in effective hepatocyte gene silencing following s.c administration.

Keywords: Drug delivery; Lipid nanoparticles; Liposomes; Nanomedicine; Subcutaneous administration; siRNA.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Chemistry, Pharmaceutical
  • Drug Delivery Systems
  • Factor VII / pharmacology
  • Female
  • Gene Silencing / drug effects*
  • Hepatocytes / drug effects*
  • Infusions, Subcutaneous
  • Lipids / chemistry*
  • Mice
  • Mice, Inbred C57BL
  • Nanoparticles / chemistry*
  • RNA, Small Interfering / administration & dosage*
  • RNA, Small Interfering / pharmacokinetics
  • RNA, Small Interfering / pharmacology*
  • Tissue Distribution

Substances

  • Lipids
  • RNA, Small Interfering
  • Factor VII