Visualization of a substrate-induced productive conformation of the catalytic triad of the Neisseria meningitidis peptidoglycan O-acetylesterase reveals mechanistic conservation in SGNH esterase family members

Acta Crystallogr D Biol Crystallogr. 2014 Oct;70(Pt 10):2631-9. doi: 10.1107/S1399004714016770. Epub 2014 Sep 27.

Abstract

Peptidoglycan O-acetylesterase (Ape1), which is required for host survival in Neisseria sp., belongs to the diverse SGNH hydrolase superfamily, which includes important viral and bacterial virulence factors. Here, multi-domain crystal structures of Ape1 with an SGNH catalytic domain and a newly identified putative peptidoglycan-detection module are reported. Enzyme catalysis was performed in Ape1 crystals and key catalytic intermediates along the SGNH esterase hydrolysis reaction pathway were visualized, revealing a substrate-induced productive conformation of the catalytic triad, a mechanistic detail that has not previously been observed. This substrate-induced productive conformation of the catalytic triad shifts the established dogma on these enzymes, generating valuable insight into the structure-based design of drugs targeting the SGNH esterase superfamily.

Keywords: Ape1; SGNH hydrolase superfamily; peptidoglycan O-acetylesterase.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins / chemistry
  • Bacterial Proteins / metabolism
  • Catalytic Domain
  • Crystallography, X-Ray
  • Esterases / chemistry*
  • Esterases / metabolism*
  • Models, Molecular
  • Neisseria meningitidis / chemistry*
  • Peptidoglycan / metabolism
  • Protein Conformation

Substances

  • Bacterial Proteins
  • Peptidoglycan
  • Esterases

Associated data

  • PDB/4K3U
  • PDB/4K40
  • PDB/4K7J
  • PDB/4K9S