In vitro longevity of bonding properties of universal adhesives to dentin

Oper Dent. 2015 May-Jun;40(3):282-92. doi: 10.2341/14-055-L. Epub 2014 Nov 18.

Abstract

Purpose: To evaluate the immediate and 6-month resin-dentin bond strength (μTBS) and nanoleakage (NL) of universal adhesives that contain or do not contain methacryloyloxydecyl dihydrogen phosphate (MDP) and are used in the etch-and-rinse and self-etch strategies.

Methods and materials: Forty caries-free extracted third molars were divided into eight groups for μTBS (n=5). The groups were bonded with the Clearfil SE Bond (CSE) and Adper Single Bond 2 (SB) as controls; Peak Universal, self-etch (PkSe) and etch-and rinse (PkEr); Scotchbond Universal Adhesive, self-etch (ScSe) and etch-and-rinse (ScEr); and All Bond Universal, self-etch (AlSe) and etch-and-rinse (AlEr). After composite restorations, specimens were longitudinally sectioned to obtain resin-dentin bonded sticks (0.8 mm(2)). The μTBS of the specimens was tested immediately (IM) or after 6 months of water storage (6M) at 0.5 mm/min. Some sticks at each storage period were immersed in silver nitrate and photo developed, and the NL was evaluated with scanning electron microscopy. Data were analyzed with two-way repeated-measures analysis of variance and Tukey test (α=0.05).

Results: At the IM period, PkSe and PkEr showed μTBS similar to the control adhesives (p>0.05) but increased NL pattern and lower μTBS after 6M (p<0.05). ScSe and ScEr showed intermediary μTBS values at the IM period but remained stable after 6 months (p>0.05). AlSe showed the lowest μTBS (p<0.05), but μTBS and NL remained stable after 6M (p>0.05). AlEr showed higher IM μTBS but showed higher degradation after 6M (p<0.05).

Conclusions: Universal adhesives that contain MDP showed higher and more stable μTBS with reduced NL at the interfaces after 6 months of water storage.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Dental Bonding / methods*
  • Dental Bonding / standards
  • Dental Cements / standards
  • Dental Cements / therapeutic use
  • Dental Etching / methods
  • Dental Etching / standards
  • Dental Stress Analysis
  • Dentin / metabolism*
  • Dentin-Bonding Agents / standards
  • Dentin-Bonding Agents / therapeutic use*
  • Humans
  • In Vitro Techniques
  • Molar
  • Resin Cements / standards
  • Resin Cements / therapeutic use
  • Tensile Strength
  • Time Factors

Substances

  • Adper single bond 2
  • Clearfil SE Bond
  • Dental Cements
  • Dentin-Bonding Agents
  • Resin Cements
  • Scotchbond