Laser-assisted high-pressure-induced polymerization of 2-(hydroxyethyl)methacrylate

J Phys Chem B. 2015 Feb 26;119(8):3577-82. doi: 10.1021/jp511630p. Epub 2015 Feb 11.

Abstract

We report on a successful room-temperature polymerization of 2-(hydroxyethyl)methacrylate (HEMA) under high pressure. The polymerization is observed in a limited range of pressures 0.1 to 1.6 GPa without the use of any initiator. When the compressed sample is irradiated at 488 or 355 nm by a laser, the polymerization reaction rate is increased by a factor of 10 or 30, respectively. Moreover, the shift of the laser wavelength to the UV improves the polymerization yield of the recovered sample to 84%. The catalysis of the polymerization process by light results from a one-photon-assisted electron transfer to π* antibonding states of the monomer molecule. The observed polymerization is irreversible and almost complete, which makes this synthesis process suitable for applications.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Catalysis
  • Electrons
  • Kinetics
  • Lasers
  • Methacrylates / chemistry*
  • Photons
  • Polymerization
  • Pressure
  • Spectrum Analysis, Raman
  • Temperature
  • Ultraviolet Rays

Substances

  • Methacrylates
  • hydroxyethyl methacrylate