Phosphoramidate-based peptidomimetic inhibitors of membrane type-1 matrix metalloproteinase

J Enzyme Inhib Med Chem. 2016;31(1):167-71. doi: 10.3109/14756366.2015.1010528. Epub 2015 Sep 4.

Abstract

Membrane-type I matrix metalloproteinases (MT1-MMP) is an enzyme critical to the remodeling and homeostasis of extracellular matrix, and when over expressed it contributes to metastasis and cancer cell progression. Because of its role and implication as a biomarker that is upregulated in various cancers, MT1-MMP has become an attractive target for drug discovery. A small pilot library of peptidomimetics containing a phosphoramidate core as a zinc-binding group was synthesized and tested for inhibitory potency against MT1-MMP. From this library, a novel two residue peptidomimetic scaffold was identified that confers potency against MT1-MMP at submicromolar concentrations. The results of this study confirm that for this scaffold, valine is favored as a P1 residue and leucine in the P1' position. Furthermore, steric tolerance was observed for the N-terminus, thus implicating that a second-generation library could be constructed to extend the scaffold to P2 without concomitant loss of affinity within the MT1-MMP catalytic domain.

Keywords: Inhibitor; MMP1; MT1-MMP; phosphoramidate.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Amides / chemical synthesis
  • Amides / chemistry
  • Amides / pharmacology*
  • Biocatalysis
  • Dose-Response Relationship, Drug
  • Humans
  • Matrix Metalloproteinase 14 / metabolism*
  • Matrix Metalloproteinase Inhibitors / chemical synthesis
  • Matrix Metalloproteinase Inhibitors / chemistry
  • Matrix Metalloproteinase Inhibitors / pharmacology*
  • Molecular Structure
  • Peptidomimetics / antagonists & inhibitors*
  • Peptidomimetics / metabolism
  • Phosphoric Acids / chemical synthesis
  • Phosphoric Acids / chemistry
  • Phosphoric Acids / pharmacology*
  • Recombinant Proteins / metabolism
  • Structure-Activity Relationship

Substances

  • Amides
  • Matrix Metalloproteinase Inhibitors
  • Peptidomimetics
  • Phosphoric Acids
  • Recombinant Proteins
  • phosphoramidic acid
  • Matrix Metalloproteinase 14