Reversible, time-dependent inhibition of CYP3A-mediated metabolism of midazolam and tacrolimus by telaprevir in human liver microsomes

J Pharm Pharm Sci. 2015;18(1):101-11. doi: 10.18433/j3288c.

Abstract

Purpose: Telaprevir inhibits CYP3A resulting in drug-drug interactions (DDI) of unprecedented magnitude. We investigated the mechanisms by which telaprevir inhibits the oxidation of midazolam and tacrolimus in human liver microsomes (HLM).

Methods: We performed a static mechanistic DDI prediction to evaluate whether previously reported competitive inhibition of CYP3A by telaprevir and its diastereomeric metabolite - VRT-127394 is sufficient to explain the remarkable reduction in oral clearance observed with oral midazolam and tacrolimus. To further explore the inhibitory mechanisms of telaprevir, we assessed whether telaprevir-mediated inhibition of the oxidation of midazolam and tacrolimus is time-dependent in human liver microsomes, and whether any observed time-dependency was irreversible or reversible in nature.

Results: The competitive inhibition model failed to account for the magnitude of telaprevir interactions in human subjects. In comparing HLM incubations with and without a prior 30-min exposure to telaprevir, a respective 4- and 11-fold reduction in IC50 was observed with midazolam and tacrolimus as substrates. This time-dependent inhibition was shown to be NADPH-dependent. Upon dilution of microsomes following pre-incubation with telaprevir, time-dependent inhibition of midazolam metabolism was completely reversed, whereas partial reversal occurred with tacrolimus.

Conclusions: The interaction between telaprevir and midazolam or tacrolimus involves both competitive and time-dependent inhibition. The time-dependent component is not explained by irreversible inactivation of CYP3A. Formation of potent inhibitory metabolites may contribute to the remarkable in vivo inhibitory potency of telaprevir.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antiviral Agents / administration & dosage
  • Antiviral Agents / pharmacology
  • Cytochrome P-450 CYP3A / drug effects
  • Cytochrome P-450 CYP3A / metabolism*
  • Cytochrome P-450 CYP3A Inhibitors / administration & dosage
  • Cytochrome P-450 CYP3A Inhibitors / pharmacology
  • Drug Interactions
  • Humans
  • Immunosuppressive Agents / administration & dosage
  • Immunosuppressive Agents / metabolism
  • Inhibitory Concentration 50
  • Microsomes, Liver / drug effects
  • Microsomes, Liver / enzymology
  • Midazolam / administration & dosage
  • Midazolam / metabolism*
  • NADP / metabolism
  • Oligopeptides / administration & dosage
  • Oligopeptides / pharmacology*
  • Tacrolimus / administration & dosage
  • Tacrolimus / metabolism*
  • Time Factors

Substances

  • Antiviral Agents
  • Cytochrome P-450 CYP3A Inhibitors
  • Immunosuppressive Agents
  • Oligopeptides
  • NADP
  • telaprevir
  • Cytochrome P-450 CYP3A
  • Midazolam
  • Tacrolimus