Aluminium-phthalocyanine chloride nanoemulsions for anticancer photodynamic therapy: Development and in vitro activity against monolayers and spheroids of human mammary adenocarcinoma MCF-7 cells

J Nanobiotechnology. 2015 May 13:13:36. doi: 10.1186/s12951-015-0095-3.

Abstract

Background: Photodynamic therapy (PDT) combines light, molecular oxygen and a photosensitizer to induce oxidative stress in target cells. Certain hydrophobic photosensitizers, such as aluminium-phthalocyanine chloride (AlPc), have significant potential for antitumor PDT applications. However, hydrophobic molecules often require drug-delivery systems, such as nanostructures, to improve their pharmacokinetic properties and to prevent aggregation, which has a quenching effect on the photoemission properties in aqueous media. As a result, this work aims to develop and test the efficacy of an AlPc in the form of a nanoemulsion to enable its use in anticancer PDT.

Results: The nanoemulsion was developed using castor oil and Cremophor ELP®, and a monodisperse population of nanodroplets with a hydrodynamic diameter of approximately 25 nm was obtained. While free AlPc failed to show significant activity against human breast adenocarcinoma MCF-7 cells in an in vitro PDT assay, the AlPc in the nanoemulsion showed intense photodynamic activity. Photoactivated AlPc exhibited a 50 % cytotoxicity concentration (CC50) of 6.0 nM when applied to MCF-7 cell monolayers and exerted a powerful cytotoxic effect on MCF-7 cell spheroids.

Conclusion: Through the use of spontaneous emulsification, a stable AlPc nanoemulsion was developed that exhibits strong in vitro photodynamic activity on cancer cells.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aluminum / chemistry*
  • Aluminum / pharmacology
  • Antineoplastic Agents / chemistry
  • Antineoplastic Agents / pharmacology*
  • Castor Oil / chemistry
  • Colloids / chemistry
  • Dose-Response Relationship, Drug
  • Drug Delivery Systems
  • Emulsions / chemistry*
  • Emulsions / pharmacology
  • Humans
  • Indoles / chemistry*
  • Indoles / pharmacology
  • Isoindoles
  • MCF-7 Cells / drug effects
  • MCF-7 Cells / pathology
  • Nanostructures / chemistry
  • Photochemotherapy / methods*
  • Spectrum Analysis, Raman
  • Surface-Active Agents / chemistry

Substances

  • Antineoplastic Agents
  • Colloids
  • Emulsions
  • Indoles
  • Isoindoles
  • Surface-Active Agents
  • Castor Oil
  • Aluminum
  • phthalocyanine