The radiosensitizing activity of the SMAC-mimetic, Debio 1143, is TNFα-mediated in head and neck squamous cell carcinoma

Radiother Oncol. 2015 Sep;116(3):495-503. doi: 10.1016/j.radonc.2015.05.017. Epub 2015 Jun 18.

Abstract

Background and purpose: Second mitochondria-derived activator of caspase (SMAC)-mimetics are a new class of targeted drugs that specifically induce apoptotic cancer cell death and block pro-survival signaling by antagonizing selected members of the inhibitor of apoptosis protein (IAP) family.

Material and methods: The present study was designed to investigate the radiosensitizing effect and optimal sequence of administration of the novel SMAC-mimetic Debio 1143 in vitro and in vivo. Apoptosis, alteration of DNA damage repair (DDR), and tumor necrosis factor-alpha (TNF-α) signaling were examined.

Results: In vitro, Debio 1143 displayed anti-proliferative activity and enhanced intrinsic radiation sensitivity in 5/6 head and neck squamous cell carcinoma (HNSCC) cell lines in a synergistic manner. In vivo, Debio 1143 dose-dependently radio-sensitized FaDu and SQ20B xenografts, resulting in complete tumor regression in 8/10 FaDu-xenografted mice at the high dose level. At the molecular level, Debio 1143 combined with radiotherapy (RT) induced enhancement of caspase-3 activity, increase in Annexin V-positive cells and karyopyknosis, and increase in TNF-α mRNA levels. Finally, in a neutralization experiment using a TNF-α-blocking antibody and a caspase inhibitor, it was shown that the radiosensitizing effect of Debio 1143 is mediated by caspases and TNF-α.

Conclusions: These results demonstrate that the novel SMAC-mimetic Debio 1143 is a radiosensitizing agent that is worthy of further investigation in clinical trials in combination with radiotherapy.

Keywords: HNSCC; IAP inhibitor; Radiosensitizer; SMAC-mimetic.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Antineoplastic Agents / pharmacology*
  • Apoptosis / drug effects
  • Apoptosis Regulatory Proteins
  • Azocines / pharmacology*
  • Benzhydryl Compounds / pharmacology*
  • Carcinoma, Squamous Cell / therapy*
  • Caspase 3 / metabolism
  • Cell Death / drug effects
  • Cell Line, Tumor
  • Chemoradiotherapy / methods
  • Female
  • Head and Neck Neoplasms / therapy*
  • Humans
  • Inhibitor of Apoptosis Proteins / antagonists & inhibitors
  • Intracellular Signaling Peptides and Proteins / pharmacology
  • Mice, Inbred Strains
  • Mitochondrial Proteins / pharmacology
  • Neoplasm Transplantation
  • Radiation-Sensitizing Agents / pharmacology*
  • Signal Transduction / drug effects
  • Squamous Cell Carcinoma of Head and Neck
  • Transplantation, Heterologous
  • Tumor Necrosis Factor-alpha / physiology*
  • Xenograft Model Antitumor Assays / methods

Substances

  • Antineoplastic Agents
  • Apoptosis Regulatory Proteins
  • Azocines
  • Benzhydryl Compounds
  • DIABLO protein, human
  • Inhibitor of Apoptosis Proteins
  • Intracellular Signaling Peptides and Proteins
  • Mitochondrial Proteins
  • N-benzhydryl-5-(2-(methylamino)propanamido)-3-(3-methylbutanoyl)-6-oxodecahydropyrrolo(1,2-a)(1,5)diazocine-8-carboxamide
  • Radiation-Sensitizing Agents
  • Tumor Necrosis Factor-alpha
  • Caspase 3