Differential Nanosecond Protein Dynamics in Homologous Calcium Sensors

ACS Chem Biol. 2015 Oct 16;10(10):2344-52. doi: 10.1021/acschembio.5b00278. Epub 2015 Aug 7.

Abstract

Shaping the temporal response of photoreceptors is facilitated by a well-balanced second messenger cascade, in which two neuronal Ca(2+)-sensor proteins operate in a sequential relay mechanism. Although they share structurally similar sensing units, they differentially activate the same target protein. Here, as a prototypical case in Ca(2+)-mediated signal processing, we investigate differential cellular responsiveness in protein conformational dynamics on a nanosecond time scale. For this, we have site-specifically labeled cysteine residues in guanylate cyclase-activating protein GCAP1 by the fluorescent dye Alexa647 and probed its local environment via time-resolved fluorescence spectroscopy. Fluorescence lifetime and rotational anisotropy measurements reveal a distinct structural movement of the polypeptide chain around position 106 upon release of Ca(2+). This is supported by analyzing the diffusional dye motion in a wobbling-in-a-cone model and by molecular dynamics simulations. We conclude that GCAP1 and its cellular cognate GCAP2 operate by distinctly different switching mechanisms despite their high structural homology.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Calcium / analysis*
  • Calcium / chemistry*
  • Carbocyanines / analysis
  • Fluorescent Dyes / analysis
  • Guanylate Cyclase-Activating Proteins / chemistry*
  • Molecular Dynamics Simulation
  • Protein Conformation
  • Protein Structure, Tertiary
  • Spectrometry, Fluorescence

Substances

  • Alexa Fluor 647
  • Carbocyanines
  • Fluorescent Dyes
  • Guanylate Cyclase-Activating Proteins
  • Calcium