Improvement of Topical Palmitoylethanolamide Anti-Inflammatory Activity by Pegylated Prodrugs

Mol Pharm. 2015 Sep 8;12(9):3369-79. doi: 10.1021/acs.molpharmaceut.5b00397. Epub 2015 Aug 24.

Abstract

A small library of polyethylene glycol esters of palmitoylethanolamide (PEA) was synthesized with the aim of improving the pharmacokinetic profile of the parent drug after topical administration. Synthesized prodrugs were studied for their skin accumulation, pharmacological activities, in vitro chemical stability, and in silico enzymatic hydrolysis. Prodrugs proved to be able to delay and prolong the pharmacological activity of PEA by modification of its skin accumulation profile. Pharmacokinetic improvements were particularly evident when specific structural requirements, such as flexibility and reduced molecular weight, were respected. Some of the synthesized prodrugs prolonged the pharmacological effects 5 days following topical administration, while a formulation composed by PEA and two pegylated prodrugs showed both rapid onset and long-lasting activity, suggesting the potential use of polyethylene glycol prodrugs of PEA as a suitable candidate for the treatment of skin inflammatory diseases.

Keywords: N-palmitoylethanolamide; anti-inflammatory effects; antihyperalgesic effects; pegylated prodrugs; topical delivery.

MeSH terms

  • Administration, Cutaneous
  • Administration, Topical
  • Amides
  • Animals
  • Anti-Inflammatory Agents, Non-Steroidal / chemistry
  • Anti-Inflammatory Agents, Non-Steroidal / pharmacology*
  • Dermatologic Agents / chemistry
  • Dermatologic Agents / pharmacology*
  • Drug Stability
  • Ethanolamines / chemistry
  • Ethanolamines / pharmacology*
  • Hydrolysis
  • Male
  • Mice
  • Models, Molecular
  • Palmitic Acids / chemistry
  • Palmitic Acids / pharmacology*
  • Polyethylene Glycols / chemistry*
  • Prodrugs / chemistry
  • Prodrugs / pharmacology*
  • Skin Absorption / drug effects*

Substances

  • Amides
  • Anti-Inflammatory Agents, Non-Steroidal
  • Dermatologic Agents
  • Ethanolamines
  • Palmitic Acids
  • Prodrugs
  • Polyethylene Glycols
  • palmidrol