Functional expression, purification, characterization, and membrane reconstitution of non-structural protein 2 from hepatitis C virus

Protein Expr Purif. 2015 Dec:116:1-6. doi: 10.1016/j.pep.2015.08.027. Epub 2015 Aug 29.

Abstract

Non-structural protein 2 (NS2) of the hepatitis C virus (HCV) is an integral membrane protein that contains a cysteine protease and that plays a central organizing role in assembly of infectious progeny virions. While the crystal structure of the protease domain has been solved, the NS2 full-length form remains biochemically and structurally uncharacterized because recombinant NS2 could not be prepared in sufficient quantities from cell-based systems. We show here that functional NS2 in the context of the NS2-NS3pro precursor protein, ensuring NS2-NS3 cleavage, can be efficiently expressed by using a wheat germ cell-free expression system. In this same system, we subsequently successfully produce and purify milligram amounts of a detergent-solubilized form of full-length NS2 exhibiting the expected secondary structure content. Furthermore, immuno-electron microscopy analyses of reconstituted proteoliposomes demonstrate NS2 association with model membranes.

Keywords: Cell-free protein expression; Hepatitis C virus; Lipid reconstitution; Membrane protein; Non-structural protein 2.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Sequence
  • Cell-Free System / metabolism
  • Chromatography, Gel
  • Cloning, Molecular
  • Detergents / chemistry
  • Gene Expression
  • Hepacivirus / chemistry*
  • Hepacivirus / genetics*
  • Hepatitis C / virology
  • Liposomes / chemistry
  • Membrane Lipids / chemistry
  • Molecular Sequence Data
  • Plasmids / genetics
  • Protein Structure, Secondary
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / genetics
  • Recombinant Proteins / isolation & purification
  • Solubility
  • Triticum / genetics
  • Viral Nonstructural Proteins / chemistry*
  • Viral Nonstructural Proteins / genetics*
  • Viral Nonstructural Proteins / isolation & purification

Substances

  • Detergents
  • Liposomes
  • Membrane Lipids
  • NS2 protein, Hepatitis C virus
  • Recombinant Proteins
  • Viral Nonstructural Proteins