Structural insights into conformational switching in the copper metalloregulator CsoR from Streptomyces lividans

Acta Crystallogr D Biol Crystallogr. 2015 Sep;71(Pt 9):1872-8. doi: 10.1107/S1399004715013012. Epub 2015 Aug 25.

Abstract

Copper-sensitive operon repressors (CsoRs) act to sense cuprous ions and bind them with a high affinity under copper stress in many bacteria. The binding of copper(I) leads to a conformational change in their homotetramer structure, causing disassembly of the operator DNA-CsoR complex and evoking a transcriptional response. Atomic-level structural insight into the conformational switching mechanism between the apo and metal-bound states is lacking. Here, a new X-ray crystal structure of the CsoR from Streptomyces lividans is reported and compared with a previously reported S. lividans CsoR X-ray structure crystallized under different conditions. Based on evidence from this new X-ray structure, it is revealed that the conformational switching between states centres on a concertina effect at the C-terminal end of each α2 helix in the homotetramer. This drives the Cys104 side chain, a copper(I)-ligating residue, into a position enabling copper(I) coordination and as a result disrupts the α2-helix geometry, leading to a compacting and twisting of the homotetramer structure. Strikingly, the conformational switching induces a redistribution of electrostatic surface potential on the tetrameric DNA-binding face, which in the copper(I)-bound state would no longer favour interaction with the mode of operator DNA binding.

Keywords: CsoR; allostery; copper; metalloregulator.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Bacterial Proteins / chemistry*
  • Copper / chemistry*
  • Crystallography, X-Ray
  • DNA, Bacterial / chemistry
  • Models, Molecular
  • Protein Conformation
  • Streptomyces lividans / chemistry*

Substances

  • Bacterial Proteins
  • DNA, Bacterial
  • Copper