Ocular delivery of cyanidin-3-glycoside in liposomes and its prevention of selenite-induced oxidative stress

Drug Dev Ind Pharm. 2016;42(4):546-53. doi: 10.3109/03639045.2015.1088867. Epub 2015 Sep 22.

Abstract

Context: Cataracts have become the leading cause of blindness around the world, which is mainly mediated by oxidative stress.

Objective: N-trimethyl chitosan (TMC)-coated liposomes of cyanidin-3-glycoside (C3G) (C3G-TCL) were prepared to attenuate oxidative stress induced by selenite sodium in rats.

Materials and methods: C3G-TCL were prepared by reverse-phase evaporation method and then coated with self-synthesized TMC. The physicochemical properties were determined. A gamma-scintigraphy study was employed to evaluate the precorneal elimination of the radioactive preparations. The transcorneal visualization for fluorescence-labeled samples was determined by confocal laser scanning microscopy (CLSM). The in vivo anti-oxidative study using C3G-TCL was carried out in rats with selenite-induced cataracts by topical administration.

Results: The sphere-like morphological characterization of the vesicles was confirmed by TEM, with a size of 158.3 ± 2.8 nm and a zeta potential of 31.7 mV. The encapsulation efficiency was (53.7 ± 0.2) % as measured by ultrafiltration. C3G-TCL showed a 3.3-fold increment in precorneal residence time when compared with that of the (99m)Tc-solution. A TMC coating enhanced the transepithelial transport of liposomes to a depth of 40-μm in the cornea. Moreover, C3G-TCL could significantly elevate the activity of superoxide dismutase and catalase in lens and also show a considerable reversal of reduced glutathione activity. The lipid peroxidation in lens was strongly prevented when compared with that of groups treated with uncoated C3G-loaded liposomes.

Discussion and conclusion: The coating material TMC for liposomes helps improve the anti-oxidative effect of C3G in vivo through prolonged residence time on the cornea and improved permeability in the corneal epithelium.

Keywords: Cyanidin-3-glycoside; N-trimethyl chitosan; oxidative stress; precorneal residence time; transcorneal permeability.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Anthocyanins / administration & dosage*
  • Anthocyanins / metabolism
  • Cornea / drug effects*
  • Cornea / metabolism
  • Drug Carriers / administration & dosage
  • Drug Carriers / metabolism
  • Drug Delivery Systems / methods*
  • Glycosides / administration & dosage*
  • Glycosides / metabolism
  • Liposomes
  • Oxidative Stress / drug effects*
  • Oxidative Stress / physiology
  • Rabbits
  • Rats
  • Rats, Sprague-Dawley
  • Selenious Acid / antagonists & inhibitors
  • Selenious Acid / toxicity*

Substances

  • Anthocyanins
  • Drug Carriers
  • Glycosides
  • Liposomes
  • cyanidin-3-glycoside
  • Selenious Acid