Fluorescent Analogue of Batimastat Enables Imaging of α-Secretase in Living Cells

ACS Chem Neurosci. 2016 Jan 20;7(1):40-5. doi: 10.1021/acschemneuro.5b00283. Epub 2015 Nov 18.

Abstract

The ADAM family of metalloproteases cleave a diverse range of transmembrane substrates, resulting in the release of their soluble ectodomains. This process of protein shedding, termed α-secretase processing, is involved in many facets of both normal and disease related cellular function. While the processing of substrates has been well documented, the regulation and trafficking of the ADAMs are less well understood. Tools that allow for the study of ADAMs under their native environment will allow for a better understanding of their regulation and activity. Here we describe the design and evaluation of a novel fluorescent analogue of a well-characterized ADAM inhibitor, Batimastat. This probe exhibited similar activity for inhibiting α-secretase processing in cells as did Batimastat. Importantly, this probe specifically labeled ADAMs fluorescently in both fixed and living cells, enabling the possibility to study the trafficking of α-secretase proteins in a dynamic environment.

Keywords: ADAMs; fluorescence; live-cell imaging; probe; α-secretase.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • ADAM Proteins / drug effects
  • ADAM Proteins / metabolism*
  • Amyloid Precursor Protein Secretases / genetics
  • Amyloid Precursor Protein Secretases / metabolism*
  • Amyloid beta-Protein Precursor / metabolism
  • Analysis of Variance
  • Animals
  • CHO Cells
  • Cricetulus
  • Dose-Response Relationship, Drug
  • Membrane Glycoproteins / metabolism
  • Microscopy, Fluorescence
  • Phenylalanine / analogs & derivatives*
  • Phenylalanine / chemistry
  • Phenylalanine / pharmacology
  • Protease Inhibitors / chemistry
  • Protease Inhibitors / pharmacology*
  • RNA, Small Interfering / genetics
  • RNA, Small Interfering / metabolism
  • Thiophenes / chemistry
  • Thiophenes / pharmacology*
  • Transfection

Substances

  • Amyloid beta-Protein Precursor
  • Membrane Glycoproteins
  • Protease Inhibitors
  • RNA, Small Interfering
  • Thiophenes
  • nicastrin protein
  • Phenylalanine
  • batimastat
  • Amyloid Precursor Protein Secretases
  • ADAM Proteins