Solution-based routes to ammine metal borohydrides: formation of ammonia-borane

Chem Commun (Camb). 2016 Feb 11;52(12):2581-4. doi: 10.1039/c5cc10027e. Epub 2016 Jan 11.

Abstract

Ammine metal borohydrides (AMBs) have recently commanded attention as low-temperature hydrogen sources. As an alternative to widely used mechanochemical synthesis that affords mixtures with salt co-products, we have been investigating solution synthesis routes to obtain pure AMBs. Here we show that reactions of MCln + nNaBH4 with ammonia in thf afford ammonia-borane (AB) via borane abstraction from M-coordinated borohydride. The amount of AB formed correlates roughly with the metal ion electronegativity and AMB thermal stability, except for reducible metals such as Ti, which affords nearly 3 equiv. of AB per Ti.

Publication types

  • Research Support, Non-U.S. Gov't