Folate receptor-targeted multimodal polymersomes for delivery of quantum dots and doxorubicin to breast adenocarcinoma: In vitro and in vivo evaluation

Int J Pharm. 2016 Mar 16;500(1-2):162-78. doi: 10.1016/j.ijpharm.2016.01.040. Epub 2016 Jan 21.

Abstract

In this study, we report the design and delivery of tumor-targeted, quantum dot (QD) and doxorubicin (DOX)-encapsulated PEG-PLGA nanopolymersomes (NPs) for the imaging and chemotherapy of breast cancer. To achieve active cancer targeting, QD and DOX-encapsulated NPs were conjugated with folate for folate-binding protein receptor-guided delivery, which overexpressed in many cancer cells. Hydrophobic DOX and hydrophilic MSA-capped QD were encapsulated in the bilayer and core of the PEG-PLGA nanopolymersomes, respectively. The data show that the formulated NPs sustained DOX release for a period of 12 days. Fluorescence microscopy and MTT assay demonstrated that the developed folate-targeted DOX-QD NPs had higher cytotoxicity than non-targeted NPs and the free form of the drug; moreover, they preferentially accumulated in 4T1 and MCF-7 cells in vitro. In vivo experiments including whole organ tissue-homogenate analysis and organ fluorescence microscopy imaging of BALB/c mice bearing 4T1 breast adenocarcinoma showed that the folate receptor-targeted QD encapsulated NPs accumulate at tumor sites 6h following intravenous injection. Acute toxicity studies of the prepared targeted QD-loaded NPs showed no evidence of long-term harmful histopathological and physiological effects on the treated animals. The in vivo tumor inhibitory effect of folic acid (FA)-QD-DOX NPs demonstrated an augmented therapeutic efficacy of targeted formulation over the non-targeted and free drug. The data obtained illustrate a high potential of the prepared targeted theranostic nanoplatform in the treatment and imaging of breast cancer. This study may open new directions for preparation of QD-based theranostic polymersomes for clinical application.

Keywords: 4T1; Breast cancer; Doxorubicin; Nanopolymersome; PEG-PLGA; Quantum dot.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adenocarcinoma / drug therapy
  • Adenocarcinoma / metabolism
  • Adenocarcinoma / pathology
  • Animals
  • Antibiotics, Antineoplastic / administration & dosage*
  • Antibiotics, Antineoplastic / chemistry
  • Antibiotics, Antineoplastic / pharmacology
  • Breast Neoplasms / drug therapy
  • Breast Neoplasms / metabolism
  • Breast Neoplasms / pathology
  • Cadmium Compounds / administration & dosage*
  • Cadmium Compounds / chemistry
  • Cell Line, Tumor
  • Cell Survival / drug effects
  • Doxorubicin / administration & dosage*
  • Doxorubicin / chemistry
  • Doxorubicin / pharmacology
  • Drug Delivery Systems
  • Drug Liberation
  • Folic Acid / administration & dosage*
  • Folic Acid / chemistry
  • Folic Acid / pharmacology
  • Folic Acid Transporters / metabolism
  • Humans
  • Mice
  • Mice, Inbred BALB C
  • Microscopy, Electron, Transmission
  • NIH 3T3 Cells
  • Polyesters / administration & dosage*
  • Polyesters / chemistry
  • Polyesters / pharmacology
  • Polyethylene Glycols / administration & dosage*
  • Polyethylene Glycols / chemistry
  • Polyethylene Glycols / pharmacology
  • Quantum Dots / administration & dosage*
  • Quantum Dots / chemistry
  • Quantum Dots / ultrastructure
  • Tellurium / administration & dosage*
  • Tellurium / chemistry
  • Tumor Burden / drug effects

Substances

  • Antibiotics, Antineoplastic
  • Cadmium Compounds
  • Folic Acid Transporters
  • Polyesters
  • polyethylene glycol-poly(lactide-co-glycolide)
  • Polyethylene Glycols
  • Doxorubicin
  • Folic Acid
  • Tellurium
  • cadmium telluride