Iodixanol Gradient Centrifugation to Separate Components of the Low-Density Membrane Fraction from 3T3-L1 Adipocytes

Cold Spring Harb Protoc. 2016 Feb 1;2016(2):pdb.prot083709. doi: 10.1101/pdb.prot083709.

Abstract

We optimized a set of fractionation techniques to facilitate the isolation of subcellular compartments containing insulin-sensitive glucose transporter isoform 4 (GLUT4), which is mobilized from GLUT4 storage vesicles (GSVs) in fat and muscle cells in response to insulin. In the absence of insulin, GLUT4 undergoes a continuous cycle of GSV formation and fusion with other compartments. Full membrane fractionation of 3T3-L1 adipocytes produces a low-density membrane fraction that contains both the constitutive recycling pool (the endosomal recycling compartments) and the insulin-sensitive pool (the GSVs). These two pools can be separated based on density using iodixanol gradient centrifugation, described here.

MeSH terms

  • 3T3-L1 Cells / chemistry*
  • 3T3-L1 Cells / physiology*
  • Animals
  • Cell Fractionation / methods*
  • Centrifugation, Density Gradient / methods*
  • Membranes / chemistry*
  • Mice
  • Triiodobenzoic Acids*

Substances

  • Triiodobenzoic Acids
  • iodixanol