Anti-osteoclastogenic activity of isoliquiritigenin via inhibition of NF-κB-dependent autophagic pathway

Biochem Pharmacol. 2016 Apr 15:106:82-93. doi: 10.1016/j.bcp.2016.03.002. Epub 2016 Mar 3.

Abstract

Previous studies, including those from our laboratory, have demonstrated that the natural flavonoid isoliquiritigenin (ISL) is a promising agent for bone destructive diseases. However, the mechanisms underlying its anti-osteoclastogenic effects are still far from clear. Here, we evaluated the potential alterations of autophagy and nuclear factor-κB (NF-κB) during anti-osteoclastogenic effects by ISL in vitro and in vivo. We observed that ISL inhibited the receptor activator of nuclear factor-κB ligand (RANKL)-induced osteoclastogenesis and suppressed autophagic microtubule-associated protein light chain 3 (LC3)-II and Beclin 1 accumulation. ISL treatment resulted in the interruption of several specific features for autophagy in osteoclast precursors, including acidic vesicular organelle formation, LC3-II accumulation, and appearance of autophagic vacuoles. The RANKL-stimulated expression levels of autophagy-related genes and proteins also diminished in ISL-treated osteoclast precursors. The reactivation of autophagy by rapamycin almost reversed the ISL-elicited anti-osteoclastogenic effects. Interestingly, ISL inhibited the RANKL-stimulated NF-κB expression and nuclear translocation, whereas the NF-κB inhibitor Bay 11-7082 markedly suppressed the RANKL-induced autophagic activation. Consistent with the in vitro results, the administration of ISL could attenuate osteoclastogenic cathepsin K, autophagic LC3, and NF-κB expression to protect against inflammatory calvarial bone erosion in vivo. Our findings highlight the inhibition of NF-κB-dependent autophagy as an important mechanism of ISL-mediated anti-osteoclastogenic activity.

Keywords: Autophagy; Isoliquiritigenin; Lipopolysaccharide; Nuclear factor-κB; Osteoclastogenesis.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Apoptosis Regulatory Proteins / genetics
  • Apoptosis Regulatory Proteins / metabolism
  • Autophagy / drug effects*
  • Beclin-1
  • Bone Density Conservation Agents / antagonists & inhibitors
  • Bone Density Conservation Agents / pharmacology*
  • Bone Resorption / chemically induced
  • Bone Resorption / drug therapy*
  • Bone Resorption / genetics
  • Bone Resorption / pathology
  • Cathepsin K / genetics
  • Cathepsin K / metabolism
  • Cell Differentiation / drug effects
  • Cell Line
  • Chalcones / antagonists & inhibitors
  • Chalcones / pharmacology*
  • Gene Expression Regulation
  • Lipopolysaccharides
  • Macrophages / drug effects
  • Macrophages / metabolism
  • Macrophages / pathology
  • Male
  • Mice
  • Mice, Inbred BALB C
  • Microtubule-Associated Proteins / genetics
  • Microtubule-Associated Proteins / metabolism
  • NF-kappa B / antagonists & inhibitors*
  • NF-kappa B / genetics
  • NF-kappa B / metabolism
  • Nitriles / pharmacology
  • Osteoclasts / drug effects*
  • Osteoclasts / metabolism
  • Osteoclasts / pathology
  • RANK Ligand / genetics
  • RANK Ligand / metabolism
  • Signal Transduction
  • Sirolimus / pharmacology
  • Skull / drug effects
  • Skull / metabolism
  • Skull / pathology
  • Sulfones / pharmacology

Substances

  • 3-(4-methylphenylsulfonyl)-2-propenenitrile
  • Apoptosis Regulatory Proteins
  • Beclin-1
  • Becn1 protein, mouse
  • Bone Density Conservation Agents
  • Chalcones
  • Lipopolysaccharides
  • Map1lc3b protein, mouse
  • Microtubule-Associated Proteins
  • NF-kappa B
  • Nitriles
  • RANK Ligand
  • Sulfones
  • Tnfsf11 protein, mouse
  • isoliquiritigenin
  • Cathepsin K
  • Ctsk protein, mouse
  • Sirolimus