A Novel Class of Dopamine D4 Receptor Ligands Bearing an Imidazoline Nucleus

ChemMedChem. 2016 Aug 19;11(16):1819-28. doi: 10.1002/cmdc.201600022. Epub 2016 Mar 15.

Abstract

Over the years, the 2-substituted imidazoline nucleus has been demonstrated to be a bioversatile structural motif. In this study, novel imidazoline derivatives bearing a 3- and/or 4-hydroxy- or methoxy-substituted phenyl ring, linked by an ethylene bridge to position 2 of an N-benzyl- or N-phenethyl-substituted imidazoline nucleus, were prepared and studied against D2 -like receptor subtypes. Binding studies highlighted that a set of N-phenethylimidazoline compounds are selective for D4 over D2 and D3 receptors. In functional assays, the 3-methoxy-substituted derivative, endowed with the highest D4 affinity value, and its 3-hydroxy analogue behaved as partial agonists with low intrinsic efficacy and as competitive D4 antagonists when tested in the presence of the D2 -like receptor agonist quinpirole. Molecular docking analysis, performed using a homology model of the human D4 receptor developed using the X-ray crystal structure of the antagonist-bound human D3 receptor as a template, was in accordance with the binding results and provided useful information for the design of novel imidazoline D4 receptor ligands based on this new scaffold.

Keywords: D4 receptor antagonists; dopamine; drug design; imidazolines; privileged structures.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, N.I.H., Intramural

MeSH terms

  • Binding Sites / drug effects
  • Crystallography, X-Ray
  • Dose-Response Relationship, Drug
  • Drug Partial Agonism
  • HEK293 Cells
  • Humans
  • Imidazolines / chemical synthesis
  • Imidazolines / chemistry*
  • Imidazolines / pharmacology*
  • Ligands
  • Molecular Docking Simulation
  • Molecular Structure
  • Receptors, Dopamine D4 / metabolism*
  • Structure-Activity Relationship

Substances

  • Imidazolines
  • Ligands
  • Receptors, Dopamine D4