Binary-copolymer system base on low-density lipoprotein-coupled N-succinyl chitosan lipoic acid micelles for co-delivery MDR1 siRNA and paclitaxel, enhances antitumor effects via reducing drug

J Biomed Mater Res B Appl Biomater. 2017 Jul;105(5):1114-1125. doi: 10.1002/jbm.b.33636. Epub 2016 Mar 23.

Abstract

The development of effective and stable carriers of small interfering RNA (siRNA) is important for treating cancer with multidrug resistance (MDR). We developed a new gene and drug co-delivery system and checked its characteristics. Low-density lipoprotein (LDL) was coupled with N-succinyl chitosan (NSC) Lipoic acid (LA) micelles and co-delivered MDR1 siRNA and paclitaxel (PTX-siRNA/LDL-NSC-LA) to enhance antitumor effects by silencing the MDR gene of tumors (Li et al., Adv Mater 2014;26:8217-8224). In our study, we developed a new type of containing paclitaxel-loaded micelles and siRNA-loaded LDL nanoparticle. This "binary polymer" is pH and reduction dual-sensitive core-crosslinked micelles. PTX-siRNA/LDL-NSC-LA had an average particle size of (171.6 ± 6.42) nm, entrapment efficiency of (93.92 ± 1.06) %, and drug-loading amount of (12.35% ± 0.87) %. In vitro, MCF-7 cells, high expressed LDL receptor, were more sensitive to this delivery system than to taxol® and cell activity was inhibited significantly. Fluorescence microscopy showed that PTX-siRNA/LDL-NSC-LA was uptaken very conveniently and played a key role in antitumor activity. PTX-siRNA/LDL-NSC-LA protected the siRNA from degradation by macrophage phagocytosis and evidently down-regulated the level of mdr1 mRNA as well as the expression of P-gp. We tested the target ability of PTX-siRNA/LDL-NSC-LA in vivo in tumor-bearing nude mice. Results showed that this system could directly deliver siRNA and PTX to cancer cells. Thus, new co-delivering siRNA and antitumor drugs should be explored for solving MDR in cancer. © 2016 Wiley Periodicals, Inc. J Biomed Mater Res Part B: Appl Biomater, 105B: 1114-1125, 2017.

Keywords: co-delivery; low-density lipoprotein; micelles; multidrug resistance; pH-sensitive; reduction-sensitive; siRNA; tumor-targeting therapy.

MeSH terms

  • ATP Binding Cassette Transporter, Subfamily B / antagonists & inhibitors
  • ATP Binding Cassette Transporter, Subfamily B / biosynthesis
  • ATP Binding Cassette Transporter, Subfamily B / genetics
  • Animals
  • Chitosan* / chemistry
  • Chitosan* / pharmacology
  • Female
  • Gene Transfer Techniques*
  • Humans
  • Lipoproteins, LDL* / chemistry
  • Lipoproteins, LDL* / pharmacology
  • MCF-7 Cells
  • Mice
  • Mice, Nude
  • Micelles*
  • Neoplasm Proteins* / antagonists & inhibitors
  • Neoplasm Proteins* / biosynthesis
  • Neoplasm Proteins* / genetics
  • Neoplasms, Experimental* / genetics
  • Neoplasms, Experimental* / metabolism
  • Neoplasms, Experimental* / pathology
  • Neoplasms, Experimental* / therapy
  • Paclitaxel / pharmacology*
  • RNA, Small Interfering* / biosynthesis
  • RNA, Small Interfering* / genetics
  • Thioctic Acid* / chemistry
  • Thioctic Acid* / pharmacology
  • Xenograft Model Antitumor Assays

Substances

  • ABCB1 protein, human
  • ATP Binding Cassette Transporter, Subfamily B
  • Lipoproteins, LDL
  • Micelles
  • Neoplasm Proteins
  • RNA, Small Interfering
  • Thioctic Acid
  • Chitosan
  • Paclitaxel