Large-Scale Overproduction and Purification of Recombinant Histone Deacetylase 8 (HDAC8) from the Human-Pathogenic Flatworm Schistosoma mansoni

Methods Mol Biol. 2016:1436:109-18. doi: 10.1007/978-1-4939-3667-0_8.

Abstract

Epigenetic mechanisms underlie the morphological transformations and shifts in virulence of eukaryotic pathogens. The targeting of epigenetics-driven cellular programs thus represents an Achilles' heel of human parasites. Today, zinc-dependent histone deacetylases (HDACs) belong to the most explored epigenetic drug targets in eukaryotic parasites. Here, we describe an optimized protocol for the large-scale overproduction and purification of recombinant smHDAC8, an emerging epigenetic drug target in the multicellular human-pathogenic flatworm Schistosoma mansoni. The strategy employs the robustness of recombinant expression in Escherichia coli together with initial purification through a poly-histidine affinity tag that can be removed by the thrombin protease. This protocol is divided into two steps: (1) large-scale production of smHDAC8 in E. coli, and (2) purification of the target smHDAC8 protein through multiple purification steps.

Keywords: Enzyme; Histone deacetylase; Purification; Recombinant expression; Schistosoma.

MeSH terms

  • Animals
  • Epigenesis, Genetic
  • Escherichia coli / genetics
  • Escherichia coli / growth & development
  • Histone Deacetylases / genetics*
  • Histone Deacetylases / metabolism
  • Humans
  • Organisms, Genetically Modified
  • Protein Engineering / methods*
  • Recombinant Proteins / genetics
  • Recombinant Proteins / metabolism
  • Repressor Proteins / genetics*
  • Repressor Proteins / metabolism
  • Schistosoma mansoni / genetics*

Substances

  • Recombinant Proteins
  • Repressor Proteins
  • HDAC8 protein, human
  • Histone Deacetylases