Discovery of a Selective Covalent Inhibitor of Lysophospholipase-like 1 (LYPLAL1) as a Tool to Evaluate the Role of this Serine Hydrolase in Metabolism

ACS Chem Biol. 2016 Sep 16;11(9):2529-40. doi: 10.1021/acschembio.6b00266. Epub 2016 Jul 19.

Abstract

Lysophospholipase-like 1 (LYPLAL1) is an uncharacterized metabolic serine hydrolase. Human genome-wide association studies link variants of the gene encoding this enzyme to fat distribution, waist-to-hip ratio, and nonalcoholic fatty liver disease. We describe the discovery of potent and selective covalent small-molecule inhibitors of LYPLAL1 and their use to investigate its role in hepatic metabolism. In hepatocytes, selective inhibition of LYPLAL1 increased glucose production supporting the inference that LYPLAL1 is a significant actor in hepatic metabolism. The results provide an example of how a selective chemical tool can contribute to evaluating a hypothetical target for therapeutic intervention, even in the absence of complete biochemical characterization.

MeSH terms

  • Animals
  • Crystallization
  • Crystallography, X-Ray
  • Enzyme Inhibitors / pharmacology
  • Humans
  • Hydrolases / metabolism*
  • Lysophospholipase / antagonists & inhibitors*
  • Lysophospholipase / chemistry
  • Serine / metabolism*

Substances

  • Enzyme Inhibitors
  • Serine
  • Hydrolases
  • Lysophospholipase
  • LYPLAL1 protein, human