Second-Generation Non-Covalent NAAA Inhibitors are Protective in a Model of Multiple Sclerosis

Angew Chem Int Ed Engl. 2016 Sep 5;55(37):11193-11197. doi: 10.1002/anie.201603746. Epub 2016 Jul 12.

Abstract

Palmitoylethanolamide (PEA) and oleoylethanolamide (OEA) are endogenous lipid mediators that suppress inflammation. Their actions are terminated by the intracellular cysteine amidase, N-acylethanolamine acid amidase (NAAA). Even though NAAA may offer a new target for anti-inflammatory therapy, the lipid-like structures and reactive warheads of current NAAA inhibitors limit the use of these agents as oral drugs. A series of novel benzothiazole-piperazine derivatives that inhibit NAAA in a potent and selective manner by a non-covalent mechanism are described. A prototype member of this class (8) displays high oral bioavailability, access to the central nervous system (CNS), and strong activity in a mouse model of multiple sclerosis (MS). This compound exemplifies a second generation of non-covalent NAAA inhibitors that may be useful in the treatment of MS and other chronic CNS disorders.

Keywords: N-acylethanolamine acid amidase; cysteine hydrolase; fatty acylethanolamides; multiple sclerosis; neuroinflammation.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Administration, Oral
  • Amides
  • Amidohydrolases / antagonists & inhibitors*
  • Amidohydrolases / metabolism
  • Animals
  • Disease Models, Animal*
  • Dose-Response Relationship, Drug
  • Endocannabinoids / administration & dosage
  • Endocannabinoids / chemistry
  • Endocannabinoids / pharmacology*
  • Enzyme Inhibitors / administration & dosage
  • Enzyme Inhibitors / chemistry
  • Enzyme Inhibitors / pharmacology*
  • Ethanolamines / administration & dosage
  • Ethanolamines / chemistry
  • Ethanolamines / pharmacology*
  • Mice
  • Molecular Structure
  • Multiple Sclerosis / drug therapy*
  • Multiple Sclerosis / metabolism
  • Oleic Acids / administration & dosage
  • Oleic Acids / chemistry
  • Oleic Acids / pharmacology*
  • Palmitic Acids / administration & dosage
  • Palmitic Acids / chemistry
  • Palmitic Acids / pharmacology*
  • Structure-Activity Relationship

Substances

  • Amides
  • Endocannabinoids
  • Enzyme Inhibitors
  • Ethanolamines
  • Oleic Acids
  • Palmitic Acids
  • oleoylethanolamide
  • palmidrol
  • Amidohydrolases
  • NAAA protein, human