In Vitro Neuroprotective and Anti-Inflammatory Activities of Natural and Semi-Synthetic Spirosteroid Analogues

Molecules. 2016 Jul 29;21(8):992. doi: 10.3390/molecules21080992.

Abstract

Two spirosteroid analogues were synthesized and evaluated for their in vitro neuroprotective activities in PC12 cells, against glutamate-induced excitotoxicity and mitochondrial damage in glucose deprivation conditions, as well as their anti-inflammatory potential in LPS/IFNγ-stimulated microglia primary cultures. We also evaluated the in vitro anti-excitotoxic and anti-inflammatory activities of natural and endogenous steroids. Our results show that the plant-derived steroid solasodine decreased PC12 glutamate-induced excitotoxicity, but not the cell death induced by mitochondrial damage and glucose deprivation. Among the two synthetic spirosteroid analogues, only the (25R)-5α-spirostan-3,6-one (S15) protected PC12 against ischemia-related in vitro models and inhibited NO production, as well as the release of IL-1β by stimulated primary microglia. These findings provide further insights into the role of specific modifications of the A and B rings of sapogenins for their neuroprotective potential.

Keywords: excitotoxicity; inflammatory mediators; neuroprotection; spirosteroids.

MeSH terms

  • Animals
  • Anti-Inflammatory Agents* / chemical synthesis
  • Anti-Inflammatory Agents* / chemistry
  • Anti-Inflammatory Agents* / pharmacology
  • Cell Death / drug effects
  • Cell Hypoxia / drug effects
  • Female
  • Interleukin-1beta / biosynthesis
  • Microglia / metabolism*
  • Microglia / pathology
  • Mitochondria / metabolism
  • Mitochondria / pathology
  • Neuroprotective Agents* / chemical synthesis
  • Neuroprotective Agents* / chemistry
  • Neuroprotective Agents* / pharmacology
  • Nitric Oxide / biosynthesis
  • PC12 Cells
  • Rats
  • Spiro Compounds* / chemical synthesis
  • Spiro Compounds* / chemistry
  • Spiro Compounds* / pharmacology
  • Steroids* / chemical synthesis
  • Steroids* / chemistry
  • Steroids* / pharmacology

Substances

  • Anti-Inflammatory Agents
  • IL1B protein, rat
  • Interleukin-1beta
  • Neuroprotective Agents
  • Spiro Compounds
  • Steroids
  • Nitric Oxide