3,3',5,5'-Tetramethylbenzidine Oxidation on Paper Devices for Horseradish Peroxidase-based Assays

Anal Sci. 2016;32(8):815-8. doi: 10.2116/analsci.32.815.

Abstract

We report on the colorimetric oxidation of 3,3',5,5'-tetramethylbenzidine (TMB) by hydrogen peroxide using horseradish peroxidase on photolithography-fabricated (P-PAD) and wax-printed (W-PAD) paper-based analytical devices. Fabricating PADs via photolithography exposes the hydrophilic areas to polymers (photoresists) and solvents, not only reducing the hydrophilicity, but also affecting the TMB-H2O2 assay system with an unavoidable incomplete elimination of photoresist during fabrication. Detection signals are then observed in the presence of photoresist residues on the P-PAD, even at a blank HRP concentration.

MeSH terms

  • Benzidines / chemistry*
  • Colorimetry / methods
  • Horseradish Peroxidase / analysis*
  • Lab-On-A-Chip Devices
  • Oxidation-Reduction
  • Paper*

Substances

  • Benzidines
  • 3,3',5,5'-tetramethylbenzidine
  • Horseradish Peroxidase