A Panel of TrpB Biocatalysts Derived from Tryptophan Synthase through the Transfer of Mutations that Mimic Allosteric Activation

Angew Chem Int Ed Engl. 2016 Sep 12;55(38):11577-81. doi: 10.1002/anie.201606242. Epub 2016 Aug 11.

Abstract

Naturally occurring enzyme homologues often display highly divergent activity with non-natural substrates. Exploiting this diversity with enzymes engineered for new or altered function, however, is laborious because the engineering must be replicated for each homologue. A small set of mutations of the tryptophan synthase β-subunit (TrpB) from Pyrococcus furiosus, which mimics the activation afforded by binding of the α-subunit, was demonstrated to have a similar activating effect in different TrpB homologues with as little as 57 % sequence identity. Kinetic and spectroscopic analyses indicate that the mutations function through the same mechanism: mimicry of α-subunit binding. From these enzymes, we identified a new TrpB catalyst that displays a remarkably broad activity profile in the synthesis of 5-substituted tryptophans. This demonstrates that allosteric activation can be recapitulated throughout a protein family to explore natural sequence diversity for desirable biocatalytic transformations.

Keywords: allostery; enzymes; protein engineering; tryptophan synthase.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Allosteric Regulation
  • Biocatalysis
  • Kinetics
  • Mutagenesis, Site-Directed
  • Protein Binding
  • Protein Engineering
  • Protein Subunits / chemistry
  • Protein Subunits / genetics
  • Protein Subunits / metabolism
  • Pyrococcus furiosus / enzymology
  • Tryptophan Synthase / chemistry
  • Tryptophan Synthase / genetics*
  • Tryptophan Synthase / metabolism*

Substances

  • Protein Subunits
  • Tryptophan Synthase