Synthesis of maltodextrin-grafted-cinnamic acid and evaluation on its ability to stabilize anthocyanins via microencapsulation

J Microencapsul. 2016 Sep;33(6):554-562. doi: 10.1080/02652048.2016.1223201.

Abstract

In this work, maltodextrin-grafted-cinnamic acid (MD-g-CA) was synthesised and used as wall material to improve the stability of purple sweet potato anthocyanins (PSPa) via microencapsualtion. MD-g-CA was prepared through esterification in a two-step convenient synthesis procedure and characterised using infra-red (IR) spectroscopy. The IR data indicated the typical ester carbonyl stretching at around 1721 cm-1. Moreover, MD-g-CA could give about 40% inhibition of DPPH radical and present excellent UV-absorption, which were notably better than that of native MD. Maltodextrin (MD) and MD-g-CA were used to prepare PSPa microcapsules by spray drying. The stability of PSPa was evaluated by UV-Vis analysis. The microcapsules produced by MD-g-CA showed a spheres-like appearance with some cracks. Storage tests revealed that the degradation rate of PSPa embedded by MD-g-CA was much lower than that of free PSPa under the same condition. Thus, MD-g-CA could be used as an effective wall material to improve stability of anthocyanins.

Keywords: Microencapsulation; cinnamic acid; maltodextrin; purple potato anthocyanins; spray drying; stability.

MeSH terms

  • Anthocyanins / chemistry*
  • Capsules
  • Cinnamates* / chemical synthesis
  • Cinnamates* / chemistry
  • Drug Stability
  • Ipomoea batatas / chemistry
  • Polysaccharides* / chemical synthesis
  • Polysaccharides* / chemistry

Substances

  • Anthocyanins
  • Capsules
  • Cinnamates
  • Polysaccharides
  • cinnamic acid
  • maltodextrin