Sepiolite as a promising nanoclay for nano-biocomposites based on starch and biodegradable polyester

Mater Sci Eng C Mater Biol Appl. 2017 Jan 1;70(Pt 1):296-302. doi: 10.1016/j.msec.2016.08.077. Epub 2016 Aug 31.

Abstract

The effects of sepiolite addition (0, 1, 3 and 5wt%) were evaluated on dynamic-mechanical behaviour, water uptake, thermal and optical properties of thermoplastic starch (TPS)/poly (butylene adipate-co-terephthalate) (PBAT) nano-biocomposites, with different TPS/PBAT (w/w) ratios and nanofiller contents. The results highlighted the improvement of the dynamic-mechanical behaviour with the addition of sepiolite, producing high performance materials. An increase of 25°C in the Tg of TPS was recorded by DMTA analysis at sepiolite content of 5wt%. The sepiolite influenced the crystallisation of nano-biocomposites, without causing interference in the crystal organisation, evidenced by DSC analysis. The addition of sepiolite nanoclay decreased the water adsorption rate and water adsorption capacity of the corresponding nano-biocomposites. For such multiphase systems, the successful use of natural sepiolite brought a clear benefit, without the need of any modifications or additional processes to produce advanced nano-biocomposites.

Keywords: Biobased materials; Dynamic-mechanical properties; Nanoclay; Poly (butylene adipate-co-terephthalate); Thermoplastic starch.

MeSH terms

  • Adsorption
  • Aluminum Silicates / chemistry*
  • Biocompatible Materials / chemistry*
  • Calorimetry, Differential Scanning
  • Clay
  • Color
  • Elastic Modulus
  • Magnesium Silicates / chemistry*
  • Models, Theoretical
  • Nanoparticles / chemistry*
  • Polyesters / chemistry*
  • Starch / chemistry*
  • Temperature
  • Water / chemistry

Substances

  • Aluminum Silicates
  • Biocompatible Materials
  • Magnesium Silicates
  • Polyesters
  • poly(butylene adipate-co-butylene terephthalate)
  • Water
  • Starch
  • magnesium trisilicate
  • Clay