Purification, structural features, antioxidant and moisture-preserving activities of an exopolysaccharide from Lachnum YM262

Bioorg Med Chem Lett. 2017 Mar 1;27(5):1225-1232. doi: 10.1016/j.bmcl.2017.01.063. Epub 2017 Jan 21.

Abstract

A water-soluble exopolysaccharide, designated as LEP-2a, was isolated from Lachnum YM262 and purified by DEAE-Cellulose 52 and Sepharose CL-6B chromatographic columns. LEP-2a was a homogeneous polysaccharide, with a molecular weight of 1.52×105 Da. It was composed of mannose and galactose in a molar ratio of 20.6:1.0. Its structural features were investigated and elucidated by methylation analysis, periodate oxidation and Smith degradation, FT-IR and NMR spectroscopy. Based on obtained data, the backbone of LEP-2a consisted of 1,2-linked-α-d-mannose, 1,3-linked-α-d-mannose, 1,2,6-linked-α-d-mannose and 1,3-linked-β-d-galactose and the side chains were attached to the backbone at O-6 position of 1,2,6-linked-α-d-mannose. In vitro antioxidant activity assay proved that LEP-2a possessed significant scavenging activities on superoxide, hydroxyl and DPPH radical. Furthermore, LEP-2a had strong in vitro moisture-absorption and -retention capacities as compared to chitosan and glycerol. These results suggested that LEP-2a might have a good potential to be applied as a multifunctional cosmetic additive in cosmetics.

Keywords: Antioxidant; Lachnum exopolysaccharide; Moisture absorption; Moisture retention; Structural features.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antioxidants / chemistry*
  • Antioxidants / isolation & purification
  • Antioxidants / pharmacology
  • Ascomycota / chemistry*
  • Ascorbic Acid / chemistry
  • Chromatography, High Pressure Liquid
  • Magnetic Resonance Spectroscopy
  • Molecular Structure
  • Oxidation-Reduction / drug effects
  • Polysaccharides / chemistry*
  • Polysaccharides / isolation & purification
  • Polysaccharides / pharmacology
  • Preservatives, Pharmaceutical / chemistry
  • Preservatives, Pharmaceutical / isolation & purification
  • Preservatives, Pharmaceutical / pharmacology
  • Solubility
  • Water / chemistry*

Substances

  • Antioxidants
  • LEP-2a compound
  • Polysaccharides
  • Preservatives, Pharmaceutical
  • Water
  • Ascorbic Acid