In Silico and In Vitro Analysis of Interaction between Ximelagatran and Human Leukocyte Antigen (HLA)-DRB1*07:01

Int J Mol Sci. 2017 Mar 24;18(4):694. doi: 10.3390/ijms18040694.

Abstract

Idiosyncratic ximelagatran-induced hepatotoxicity has been reported to be associated with human leukocyte antigen (HLA)-DRB1*07:01 and ximelagatran has been reported to inhibit the binding of the ligand peptide to HLA-DRB1*07:01 in vitro. In order to predict the possible interaction modes of ximelagatran with HLA-DR molecules, in silico docking simulations were performed. Molecular dynamics (MD) simulations were also performed to predict the effect of ximelagatran on the binding mode of the ligand peptide to HLA-DRB1*07:01. A series of in silico simulations supported the inhibitory effect of ximelagatran on the binding of the ligand peptide to HLA-DRB1*07:01 in vitro. Furthermore, direct interactions of ximelagatran with HLA-DR molecules were evaluated in vitro, which supported the simulated interaction mode of ximelagatran with HLA-DRB1*07:01. These results indicated that ximelagatran directly interacts with the peptide binding groove of HLA-DRB1*07:01 and competes with the ligand peptide for the binding site, which could alter the immune response and lead to the idiosyncratic ximelagatran-induced hepatotoxicity.

Keywords: HLA (human leukocyte antigen); IDT (idiosyncratic drug toxicity); MD (molecular dynamics) simulation; hepatotoxicity; melagatran; ximelagatran.

MeSH terms

  • Azetidines / chemistry
  • Azetidines / metabolism*
  • Benzylamines / chemistry
  • Benzylamines / metabolism*
  • Binding Sites
  • Chromatography, High Pressure Liquid
  • HLA-DRB1 Chains / chemistry
  • HLA-DRB1 Chains / metabolism*
  • Humans
  • Ligands
  • Molecular Docking Simulation
  • Molecular Dynamics Simulation
  • Peptides / chemistry
  • Peptides / metabolism
  • Protein Structure, Tertiary
  • Tandem Mass Spectrometry

Substances

  • Azetidines
  • Benzylamines
  • HLA-DRB1 Chains
  • HLA-DRB1*07 antigen
  • Ligands
  • Peptides
  • ximelagatran