N-Heterocyclic carbene-stabilised arsinidene (AsH)

Chem Commun (Camb). 2017 Jun 1;53(45):6069-6072. doi: 10.1039/c7cc02628e.

Abstract

N-Heterocyclic carbene adducts of the parent arsinidene (AsH) were prepared by two different synthetic routes, either by reaction of As(SiMe3)3 with 2,2-difluoroimidazolines followed by desilylation or by reaction of [Na(dioxane)3.31][AsCO] with imidazolium chlorides.