A simple synthetic entryway into palladium cross-coupling catalysis

Chem Commun (Camb). 2017 Jul 13;53(57):7990-7993. doi: 10.1039/c7cc02487h.

Abstract

The simple synthesis of a family of palladates containing an imidazolium counterion is presented. These "ate" complexes can be easily converted into well-defined palladium-N-heterocyclic carbene (NHC) complexes. The synthetic protocols leading to the "ate" and to the Pd-NHC neutral complexes have been exemplified with various NHC ligands. The palladates prove efficient pre-catalysts enabling Suzuki-Miyaura and Mizoroki-Heck reactions.