Freeze-Drying as a Novel Biofabrication Method for Achieving a Controlled Microarchitecture within Large, Complex Natural Biomaterial Scaffolds

Adv Healthc Mater. 2017 Nov;6(21). doi: 10.1002/adhm.201700598. Epub 2017 Jul 31.

Abstract

The biofabrication of large natural biomaterial scaffolds into complex 3D shapes which have a controlled microarchitecture remains a major challenge. Freeze-drying (or lyophilization) is a technique used to generate scaffolds in planar 3D geometries. Here we report the development of a new biofabrication process to form a collagen-based scaffold into a large, complex geometry which has a large height to width ratio, and a controlled porous microarchitecture. This biofabrication process is validated through the successful development of a heart valve shaped scaffold, fabricated from a collagen-glycosaminoglycan co-polymer. Notably, despite the significant challenges in using freeze-drying to create such a structure, the resultant scaffold has a uniform, homogenous pore architecture throughout. This is achieved through optimization of the freeze-drying mold and the freezing parameters. We believe this to be the first demonstration of using freeze-drying to create a large, complex scaffold geometry with a controlled, porous architecture for natural biomaterials. This study validates the potential of using freeze-drying for development of organ-specific scaffold geometries for tissue engineering applications, which up until now might not have been considered feasible.

Keywords: collagen; freeze-drying; heart valves; scaffolds; tissue engineering.

MeSH terms

  • Aluminum / chemistry
  • Biocompatible Materials / chemistry*
  • Collagen / chemistry
  • Compressive Strength
  • Freeze Drying*
  • Glycosaminoglycans / chemistry
  • Microscopy, Electron, Scanning
  • Polymers / chemistry
  • Porosity
  • Tensile Strength
  • Thermal Conductivity
  • Tissue Engineering
  • Tissue Scaffolds / chemistry*

Substances

  • Biocompatible Materials
  • Glycosaminoglycans
  • Polymers
  • Collagen
  • Aluminum