Expression, purification, and functional analysis of an antigen-targeting fusion protein composed of CD40 ligand and the C-terminal fragment of ovalbumin

Protein Expr Purif. 2018 Feb:142:37-44. doi: 10.1016/j.pep.2017.09.015. Epub 2017 Sep 30.

Abstract

Delivering antigen via molecules specifically targeting receptors on the surface of antigen-presenting cells is a strategy to improve immune responses. In this study, an antigen-targeting fusion protein (OVA-CD40LS) composed of the C-terminal fragment of ovalbumin and the extracellular domain of mouse CD40 ligand was constructed by genetic fusion. The OVA-CD40LS and the control OVA (rOVA) genes were cloned in Escherichia coli and over-expressed as insoluble proteins. The rOVA protein was purified from the insoluble fraction of E. coli cell lysate by nickel affinity chromatography and refolded by step-wise dialysis to give a yield of 11.8 mg/L of culture. The OVA-CD40LS was purified by a 'two-round' nickel affinity and on-column protein-refolding chromatography. The yield was 528 μg/L of culture. The purified OVA-CD40LS, but not the rOVA, was able to simulate the production of pro-inflammatory cytokines and up-regulate cell surface marker proteins in mouse bone marrow-derived dendritic cells. The purified OVA-CD40LS elicited a robust immune response when injected submucosally in the oral cavity of mice. Collectively, the results indicate that the OVA-CD40LS fusion protein was biologically active, functioning as an antigen-targeting protein.

Keywords: Antigen-targeting; CD40L; Ovalbumin; Protein refolding.

MeSH terms

  • Animals
  • Antibodies / blood
  • Bone Marrow Cells / cytology
  • Bone Marrow Cells / drug effects
  • Bone Marrow Cells / immunology
  • CD40 Ligand / genetics
  • CD40 Ligand / immunology*
  • Cloning, Molecular
  • Dendritic Cells / cytology
  • Dendritic Cells / drug effects*
  • Dendritic Cells / immunology
  • Escherichia coli / genetics
  • Escherichia coli / metabolism
  • Female
  • Gene Expression
  • Immunity, Mucosal / drug effects*
  • Immunization
  • Interleukin-6 / biosynthesis
  • Mice
  • Mice, Inbred BALB C
  • Mouth Mucosa / cytology
  • Mouth Mucosa / drug effects
  • Mouth Mucosa / immunology
  • Ovalbumin / genetics
  • Ovalbumin / immunology*
  • Plasmids / chemistry*
  • Plasmids / metabolism
  • Primary Cell Culture
  • Recombinant Fusion Proteins / administration & dosage
  • Recombinant Fusion Proteins / biosynthesis*
  • Recombinant Fusion Proteins / genetics
  • Recombinant Fusion Proteins / immunology
  • Tumor Necrosis Factor-alpha / biosynthesis

Substances

  • Antibodies
  • Interleukin-6
  • Recombinant Fusion Proteins
  • Tumor Necrosis Factor-alpha
  • interleukin-6, mouse
  • CD40 Ligand
  • Ovalbumin