An inhibitory mechanism of action of a novel syringic-acid derivative on α-melanocyte-stimulating hormone (α-MSH)-induced melanogenesis

Life Sci. 2017 Dec 15:191:52-58. doi: 10.1016/j.lfs.2017.10.009. Epub 2017 Oct 7.

Abstract

Aims: To report the effects of a novel syringic-acid derivative, (R)-ethyl-2-acetamido-3-(4-hydroxy-3,5-dimethoxybenzoylthio)propanoate (EABTO), on melanin synthesis and to identify its mechanism of action in B16F1 melanoma cells.

Methods: The effects of EABTO on melanin synthesis in B16F1 cells and human epidermal melanocytes and the influence on cell-free tyrosinase activity were evaluated. EABTO-induced cellular signaling cascades were studied by western blotting.

Key findings: EABTO effectively decreased melanin synthesis in a dose-dependent manner but had no effect on cell-free tyrosinase activity. EABTO significantly decreased the expression of melanogenic enzymes such as tyrosinase, tyrosinase-related protein 1 (TRP-1), and TRP-2. EABTO decreased the amounts of phosphorylated cAMP response element-binding protein (CREB) and cyclic adenosine monophosphate (cAMP), thereby inhibiting expression of microphthalmia-associated transcription factor (MITF). Moreover, EABTO upregulated phosphorylated ERK. A specific ERK pathway inhibitor, PD98059, reduced EABTO-induced ERK phosphorylation and restored the expression of MITF and melanin content.

Significance: EABTO inhibits melanogenesis in B16F1 melanoma cells via suppression of the cAMP-CREB pathway and activation of ERK, thus decreasing expression of MITF and of melanogenic enzymes.

Keywords: ERK; MITF; Melanogenesis; Syringic-acid derivative; Tyrosinase.

MeSH terms

  • Acetylcysteine / analogs & derivatives*
  • Acetylcysteine / pharmacology
  • Animals
  • Biosynthetic Pathways / drug effects
  • Cell Line
  • Cell Line, Tumor
  • Cyclic AMP / metabolism
  • Cyclic AMP Response Element-Binding Protein / metabolism
  • Gallic Acid / analogs & derivatives*
  • Gallic Acid / pharmacology
  • Humans
  • MAP Kinase Signaling System / drug effects
  • Melanins / antagonists & inhibitors
  • Melanins / metabolism*
  • Melanocytes / drug effects*
  • Melanocytes / metabolism
  • Melanoma / metabolism
  • Mice
  • Microphthalmia-Associated Transcription Factor / metabolism
  • Monophenol Monooxygenase / metabolism
  • Oxidoreductases / metabolism
  • alpha-MSH / metabolism*

Substances

  • Cyclic AMP Response Element-Binding Protein
  • Melanins
  • Microphthalmia-Associated Transcription Factor
  • ethyl 2-acetamido-3-(4-hydroxy-3,5-dimethoxybenzoylthio)propanoate
  • alpha-MSH
  • Gallic Acid
  • Cyclic AMP
  • Oxidoreductases
  • tyrosinase-related protein-1
  • Monophenol Monooxygenase
  • Acetylcysteine