Toblerols: Cyclopropanol-Containing Polyketide Modulators of Antibiosis in Methylobacteria

Angew Chem Int Ed Engl. 2018 Jan 22;57(4):977-981. doi: 10.1002/anie.201709056. Epub 2017 Dec 18.

Abstract

Trans-AT polyketide synthases (PKSs) are a family of biosynthetically versatile modular type I PKSs that generate bioactive polyketides of impressive structural diversity. In this study, we detected, in the genome of several bacteria a cryptic, architecturally unusual trans-AT PKS gene cluster which eluded automated PKS prediction. Genomic mining of one of these strains, the model methylotroph Methylobacterium extorquens AM1, revealed unique epoxide- and cyclopropanol-containing polyketides named toblerols. Relative and absolute stereochemistry were determined by NMR experiments, chemical derivatization, and the comparison of CD data between the derivatized natural product and a synthesized model compound. Biosynthetic data suggest that the cyclopropanol moiety is generated by carbon-carbon shortening of a more extended precursor. Surprisingly, a knock-out strain impaired in polyketide production showed strong inhibitory activity against other methylobacteria in contrast to the wild-type producer. The activity was inhibited by complementation with toblerols, thus suggesting that these compounds modulate an as-yet unknown methylobacterial antibiotic.

Keywords: antibiotics; biosynthesis; cyclopropanes; genomics; polyketides.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Antibiosis
  • Enzyme Inhibitors / chemistry
  • Enzyme Inhibitors / metabolism
  • Enzyme Inhibitors / pharmacology
  • Ethers, Cyclic / chemistry*
  • Gene Deletion
  • Methylobacterium / drug effects
  • Methylobacterium / enzymology*
  • Methylobacterium / genetics
  • Multigene Family
  • Polyketide Synthases / antagonists & inhibitors
  • Polyketide Synthases / genetics
  • Polyketide Synthases / metabolism*
  • Polyketides / chemistry*
  • Polyketides / metabolism
  • Polyketides / pharmacology

Substances

  • Enzyme Inhibitors
  • Ethers, Cyclic
  • Polyketides
  • cyclopropanol
  • Polyketide Synthases