Identification of novel quinazolinedione derivatives as RORγt inverse agonist

Bioorg Med Chem. 2018 Feb 1;26(3):721-736. doi: 10.1016/j.bmc.2017.12.039. Epub 2017 Dec 28.

Abstract

Novel small molecules were synthesized and evaluated as retinoic acid receptor-related orphan receptor-gamma t (RORγt) inverse agonists for the treatment of inflammatory and autoimmune diseases. A hit compound, 1, was discovered by high-throughput screening of our compound library. The structure-activity relationship (SAR) study of compound 1 showed that the introduction of a chlorine group at the 3-position of 4-cyanophenyl moiety increased the potency and a 3-methylpentane-1,5-diamide linker is favorable for the activity. The carbazole moiety of 1 was also optimized; a quinazolinedione derivative 18i suppressed the increase of IL-17A mRNA level in the lymph node of a rat model of experimental autoimmune encephalomyelitis (EAE) upon oral administration. These results indicate that the novel quinazolinedione derivatives have great potential as orally available small-molecule RORγt inverse agonists for the treatment of Th17-driven autoimmune diseases. A U-shaped bioactive conformation of this chemotype with RORγt protein was also observed.

Keywords: EAE model; IL-17; Inverse agonist; Quinazolinedione; RORγt (retinoic acid receptor-related orphan receptor gamma t); Th17.

MeSH terms

  • Administration, Oral
  • Animals
  • Binding Sites
  • Drug Inverse Agonism
  • Encephalomyelitis, Autoimmune, Experimental / drug therapy
  • Encephalomyelitis, Autoimmune, Experimental / pathology
  • Encephalomyelitis, Autoimmune, Experimental / veterinary
  • Female
  • Humans
  • Inhibitory Concentration 50
  • Interleukin-17 / genetics
  • Interleukin-17 / metabolism
  • Jurkat Cells
  • Molecular Docking Simulation
  • Nuclear Receptor Subfamily 1, Group F, Member 3 / agonists*
  • Nuclear Receptor Subfamily 1, Group F, Member 3 / genetics
  • Nuclear Receptor Subfamily 1, Group F, Member 3 / metabolism
  • Protein Binding / drug effects
  • Protein Structure, Tertiary
  • Quinazolinones / administration & dosage
  • Quinazolinones / chemistry*
  • Quinazolinones / metabolism
  • Quinazolinones / pharmacology
  • Rats
  • Rats, Inbred Lew
  • Solubility
  • Structure-Activity Relationship
  • Th17 Cells / cytology
  • Th17 Cells / drug effects
  • Th17 Cells / metabolism

Substances

  • Interleukin-17
  • Nuclear Receptor Subfamily 1, Group F, Member 3
  • Quinazolinones