Expression and purification of a rapidly degraded protein, TMEM8B-a, in mammalian cell line

Protein Expr Purif. 2018 Nov:151:38-45. doi: 10.1016/j.pep.2018.06.002. Epub 2018 Jun 8.

Abstract

TMEM8B-a protein is the longer, predominant isoform of the TMEM8B gene product, which is a tumor metastasis suppressor in nasopharyngeal carcinoma (NPC) and lung cancer. TMEM8B-a is rapidly degraded via the proteasome pathway mediated by ezrin in many NPC and lung cancer cell lines, but TMEM8B-a is not ubiquitinated. In this study, we report the recombinant production of full-length modified TMEM8B-a in mammalian cells. We used the PiggyBac transposon system to efficiently generate normal and lung cancer cell lines with stable TMEM8B-a protein expression. 293FT cells were the best host cell line to express TMEM8B-a protein. Then, we treated the stable 293FT cell lines with various small-molecule inhibitors and demonstrated that treatment with MG-132 and bortezomib, which target the proteasome and disrupt its function, could prevent TMEM8B-a degradation and induce protein expression in 293FT cells. Finally, we utilized the combination of Twin-Strep-tag and Strep-Tactin XT resin to successfully purify the TMEM8B-a protein. The final yield was estimated to be approximately 10-20 μg of the purified TMEM8B-a per 3.0 × 108 293FT cells.

Keywords: Expression; Protein degradation; Purification; Small molecule inhibitor; TMEM8B.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bortezomib / pharmacology
  • Cell Line
  • Humans
  • Leupeptins / pharmacology
  • Membrane Proteins / biosynthesis
  • Membrane Proteins / isolation & purification*
  • Proteasome Endopeptidase Complex / metabolism
  • Proteasome Inhibitors / pharmacology
  • Protein Isoforms / biosynthesis
  • Protein Isoforms / isolation & purification
  • Proteolysis
  • Recombinant Proteins / biosynthesis
  • Recombinant Proteins / isolation & purification
  • Transfection
  • Tumor Suppressor Proteins / biosynthesis
  • Tumor Suppressor Proteins / isolation & purification*

Substances

  • Leupeptins
  • Membrane Proteins
  • Proteasome Inhibitors
  • Protein Isoforms
  • Recombinant Proteins
  • TMEM8B protein, human
  • Tumor Suppressor Proteins
  • Bortezomib
  • Proteasome Endopeptidase Complex
  • benzyloxycarbonylleucyl-leucyl-leucine aldehyde