Tandem Enzymatic Self-Assembly and Slow Release of Dexamethasone Enhances Its Antihepatic Fibrosis Effect

ACS Nano. 2018 Oct 23;12(10):9966-9973. doi: 10.1021/acsnano.8b04143. Epub 2018 Oct 8.

Abstract

Many chronic liver diseases will advance to hepatic fibrosis and, if without timely intervention, liver cirrhosis or even hepatocellular carcinoma. Anti-inflammation could be a standard therapeutic strategy for hepatic fibrosis treatment, but a "smart" strategy of hepatic fibrosis-targeted, either self-assembly or slow release of an anti-inflammation drug ( e.g., dexamethasone, Dex), has not been reported. Herein, we rationally designed a hydrogelator precursor Nap-Phe-Phe-Lys(Dex)-Tyr(H2PO3)-OH (1-Dex-P) and proposed a tandem enzymatic strategy of self-assembly and slow release of Dex, with which the precursor exhibited much stronger antihepatic fibrosis effect than Dex both in vitro and in vivo. Enzymatic and cell experiments validated that 1-Dex-P was first dephosphorylated by alkaline phosphatase to yield Nap-Phe-Phe-Lys(Dex)-Tyr-OH (1-Dex), which self-assembled into nanofiber 1-Dex. The nanofiber was then hydrolyzed by esterase to transform into nanofiber 1, accompanied by slow release of Dex. We anticipate that our "smart" tandem enzymatic strategy could be widely employed to design more sophisticated drug delivery systems to achieve enhanced therapeutic efficacy than free drugs in the future.

Keywords: dexamethasone; hepatic fibrosis; self-assembly; slow release; tandem.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkaline Phosphatase / metabolism*
  • Animals
  • Anti-Inflammatory Agents, Non-Steroidal / metabolism
  • Anti-Inflammatory Agents, Non-Steroidal / therapeutic use*
  • Ascomycota / enzymology
  • Dexamethasone / metabolism
  • Dexamethasone / therapeutic use*
  • Fibrosis / drug therapy*
  • Fibrosis / pathology
  • Inflammation / drug therapy
  • Inflammation / pathology
  • Lipase / metabolism*
  • Mice
  • Mice, Inbred C57BL

Substances

  • Anti-Inflammatory Agents, Non-Steroidal
  • Dexamethasone
  • Lipase
  • Alkaline Phosphatase