A soft x-ray-ultraviolet (SUV) beamline and diffractometer for resonant elastic scattering and ultraviolet-vacuum ultraviolet reflectance at the Singapore synchrotron light source

Rev Sci Instrum. 2018 Nov;89(11):113113. doi: 10.1063/1.5043341.

Abstract

A new beamline and a six-circle UHV diffractometer have been constructed at the Singapore Synchrotron Light Source with a broad energy coverage from 3.5 to 1500 eV. The beamline is optimized for ultraviolet-vacuum-ultraviolet optical reflectivity and resonant soft X-ray scattering with medium energy resolution over a broad energy range, achieved by using a self-focusing monochromator consisting of a plane mirror and three variable line spacing gratings. The unique character of the diffractometer comprises 4-circles in the vertical plane and 2-circles in the horizontal plane. Thirteen motions are available inside the UHV chamber with a base pressure of 1 × 10-9 mbar. Two sample holders working independently over a temperature range of 37 K-400 K are controlled by a closed-cycle cryostat, while the bottom holder inside a high field compact pulsed magnet is available for measurements requiring a magnetic field.