Using automated glycan assembly (AGA) for the practical synthesis of heparan sulfate oligosaccharide precursors

Org Biomol Chem. 2019 Feb 13;17(7):1817-1821. doi: 10.1039/c8ob02756k.

Abstract

Herein we report synthesis of complex heparan sulfate oligosaccharide precursors by automated glycan assembly using disaccharide donor building blocks. Rapid access to a hexasaccharide was achieved through iterative solid phase glycosylations on a photolabile resin using Glyconeer™, an automated oligosaccharide synthesiser, followed by photochemical cleavage and glycan purification using simple flash column chromatography.

Publication types

  • Research Support, Non-U.S. Gov't