A Cocktail Interaction Study Evaluating the Drug-Drug Interaction Potential of the Perpetrator Drug ASP8477 at Multiple Ascending Dose Levels

Clin Pharmacol Drug Dev. 2019 May;8(4):529-540. doi: 10.1002/cpdd.660. Epub 2019 Feb 7.

Abstract

ASP8477 (molecular weight 325.36 g/mol) is a fatty acid amide hydrolase inhibitor intended for the treatment of neuropathic pain. Results from in vitro studies indicated that ASP8477 is a direct inhibitor of cytochrome P450 (CYP) 2C8, 2C9, 2C19, 2D6, and 3A4 enzymes at expected efficacious concentrations, with the strongest effect on CYP2C19; a phase 1 study confirmed ASP8477 to be a CYP2C19 inhibitor. To further evaluate the interaction potential of ASP8477, a cocktail interaction study was performed using the probe substrates of the validated Inje cocktail containing losartan (CYP2C9), omeprazole (CYP2C19), dextromethorphan (CYP2D6), and midazolam (CYP3A4). Because ASP8477 shows nonlinear pharmacokinetics, 3 doses (20, 60, and 100 mg) were evaluated. This study revealed changes in exposure (area under the concentration-time curve) of the probe substrates after treatment with 20, 60, and 100 mg ASP8477, respectively, compared with substrates alone with geometric mean ratios of: midazolam, 119%, 151%, and 158%; losartan, 107%, 144%, and 190%; omeprazole, 213%, 456%, and 610%; and dextromethorphan, 138%, 340%, and 555% (with increasing doses, respectively). Overall, ASP8477 was a weak inhibitor for CYP3A4 and CYP2C9, a moderate to strong inhibitor for CYP2C19, and a weak to strong inhibitor for CYP2D6, with doses from 20 to 100 mg. This study confirmed that the Inje cocktail approach was able to detect relevant drug-drug interactions impacting further development of ASP8477 and future therapeutic use. With the approach used here, the inhibiting effect of a perpetrator drug on different CYP enzymes can be evaluated, and at different doses, thereby supporting dose recommendations for potential interactions.

Keywords: ASP8477; cytochrome P450; drug-drug interaction; inhibition; nonlinear pharmacokinetics.

Publication types

  • Clinical Trial
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Administration, Oral
  • Adult
  • Area Under Curve
  • Cytochrome P-450 CYP2C19 / metabolism
  • Cytochrome P-450 CYP2C8 / metabolism
  • Cytochrome P-450 CYP2C9 / metabolism
  • Cytochrome P-450 CYP2D6 / metabolism
  • Dextromethorphan / administration & dosage*
  • Dextromethorphan / pharmacokinetics
  • Dose-Response Relationship, Drug
  • Drug Interactions
  • Female
  • Humans
  • Losartan / administration & dosage*
  • Losartan / pharmacokinetics
  • Male
  • Midazolam / administration & dosage*
  • Midazolam / pharmacokinetics
  • Middle Aged
  • Omeprazole / administration & dosage*
  • Omeprazole / pharmacokinetics
  • Piperidines / administration & dosage*
  • Piperidines / pharmacokinetics
  • Pyridines / administration & dosage*
  • Pyridines / pharmacokinetics
  • Young Adult

Substances

  • ASP8477
  • Piperidines
  • Pyridines
  • Dextromethorphan
  • CYP2C9 protein, human
  • Cytochrome P-450 CYP2C9
  • CYP2C19 protein, human
  • CYP2C8 protein, human
  • Cytochrome P-450 CYP2C19
  • Cytochrome P-450 CYP2C8
  • Cytochrome P-450 CYP2D6
  • Losartan
  • Omeprazole
  • Midazolam