Use of site-directed mutagenesis to probe the role of Cys149 in the formation of charge-transfer transition in glyceraldehyde-3-phosphate dehydrogenase

Protein Eng. 1988 Apr;2(1):45-8. doi: 10.1093/protein/2.1.45.

Abstract

Oligonucleotide-directed mutagenesis was employed to produce mutants of the glyceraldehyde-3-phosphate dehydrogenase (GAPDH) of Escherichia coli and Bacillus stearothermophilus. Three different mutants proteins--His176----Asn, Cys149----Ser, Cys149----Gly--were isolated from one or both of the enzymes. The study of the properties of these mutants has shown that Cys149 is clearly responsible for the information of a charge-transfer transition, named the Racker band, observed during the NAD+ binding to apoGAPDH. This result excludes a similarity between the Racker band and the charge-transfer transition observed following the alkylation of GAPDH by 3-chloroacetyl pyridine-adenine dinucleotide.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Binding Sites
  • Cysteine
  • Escherichia coli / enzymology
  • Geobacillus stearothermophilus / enzymology
  • Glyceraldehyde-3-Phosphate Dehydrogenases / genetics*
  • Glyceraldehyde-3-Phosphate Dehydrogenases / metabolism
  • Mutation*

Substances

  • Glyceraldehyde-3-Phosphate Dehydrogenases
  • Cysteine