Copper-Catalyzed Aldol Reaction of Vinyl Azides with Trifluoromethyl Ketones

Org Lett. 2019 Sep 20;21(18):7324-7328. doi: 10.1021/acs.orglett.9b02616. Epub 2019 Sep 11.

Abstract

A novel and efficient aldol reaction of readily available vinyl azides with trifluoromethyl ketones by copper catalysis is developed. The reaction is proposed to go through a nucleophilic trapping of vinyl azides with trifluoromethyl ketones as a trifluoromethyl source, leading to the assembly of diverse trifluoromethylated compounds under mild conditions in satisfactory yield.