Expression, Purification, and Crystallization of HSV-1 Glycoproteins for Structure Determination

Methods Mol Biol. 2020:2060:377-393. doi: 10.1007/978-1-4939-9814-2_23.

Abstract

Herpes simplex viruses utilize glycoproteins displayed on the viral envelope to perform a variety of functions in the viral infectious cycle. Structural and functional studies of these viral glycoproteins can benefit from biochemical, biophysical, and structural analysis of purified proteins. Here, we describe a general protocol for expression and purification of viral glycoproteins from insect cells based on those developed for the HSV-1 gB and HSV-2 gH/gL ectodomains as well as the protocol for crystallization of these glycoproteins. This protocol can be used for generating milligram amounts of wild-type (WT) or mutant gB and gH/gL ectodomains or can be adapted to produce purified ectodomains of glycoproteins from HSV or other herpesviruses for biochemical and structural studies.

Keywords: Crystallography; Ectodomain; Glycoproteins; Herpes simplex viruses; Protein purification; Viral entry.

MeSH terms

  • Animals
  • Crystallography, X-Ray
  • Gene Expression*
  • Glycoproteins* / biosynthesis
  • Glycoproteins* / chemistry
  • Glycoproteins* / genetics
  • Glycoproteins* / isolation & purification
  • Herpesvirus 1, Human* / chemistry
  • Herpesvirus 1, Human* / genetics
  • Herpesvirus 1, Human* / metabolism
  • Recombinant Proteins / biosynthesis
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / genetics
  • Recombinant Proteins / isolation & purification
  • Sf9 Cells
  • Spodoptera
  • Viral Envelope Proteins* / biosynthesis
  • Viral Envelope Proteins* / chemistry
  • Viral Envelope Proteins* / genetics
  • Viral Envelope Proteins* / isolation & purification

Substances

  • Glycoproteins
  • Recombinant Proteins
  • Viral Envelope Proteins