Antimicrobial Peptide Mimetics Based on a Diphenylacetylene Scaffold: Synthesis, Conformational Analysis, and Activity

ChemMedChem. 2020 Oct 19;15(20):1932-1939. doi: 10.1002/cmdc.202000474. Epub 2020 Sep 15.

Abstract

Mimics of natural antimicrobial peptides are promising compounds to fight the rising threat of multi-drug resistant bacteria. Here we report the design, synthesis and conformational analysis of a new class of antimicrobial peptide mimetics incorporating a diphenylacetylene scaffold. Within a small set of compounds, we observe a correlation between amphiphilicity, the efficiency of partitioning into negatively charged membranes and antibacterial activity. The most amphiphilic compound, which contains four isoleucine residues and four lysine residues, displays species-selective antibacterial activity (most active against Bacillus subtills) and low haemolytic activity. Solution-phase conformational analysis of this compound indicates that a defined structure is adopted in the presence of negatively charged phospholipid membranes and aqueous 2,2,2-trifluoroethanol but not in water. A conformation model indicates that the cationic and hydrophobic functional groups are segregated. These results may inform the development of highly selective antimicrobial peptide mimetics for therapeutic applications.

Keywords: Antimicrobial peptides; Membrane-active compounds; Peptidomimetics.

MeSH terms

  • Alkynes / chemical synthesis
  • Alkynes / pharmacology*
  • Animals
  • Anti-Bacterial Agents / chemical synthesis
  • Anti-Bacterial Agents / pharmacology*
  • Bacteria / drug effects
  • Erythrocytes / drug effects
  • Hemolysis / drug effects
  • Lipid Bilayers / chemistry
  • Liposomes / chemistry
  • Microbial Sensitivity Tests
  • Molecular Conformation
  • Peptidomimetics / chemical synthesis
  • Peptidomimetics / pharmacology*
  • Rabbits

Substances

  • Alkynes
  • Anti-Bacterial Agents
  • Lipid Bilayers
  • Liposomes
  • Peptidomimetics